08-30182040-DC.pdf

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1、a Date: 4 December 2008 Origin: International Latest date for receipt of comments: 13 March 2009 Project no.: 2008/01493 Responsible committee: AW/5 Chemical analysis of milk and milk products Interested committees: Title: Draft BS ENISO 1211 Milk - Determination of fat content - Gravimetric method

2、(Reference method) Supersession information: If this document is published as a standard, the UK implementation of it will supersede BSENISO1211 : 2001 and partially supersede. NONE If you are aware of a current national standard which may be affected, please notify the secretary (contact details be

3、low). WARNING: THIS IS A DRAFT AND MUST NOT BE REGARDED OR USED AS A BRITISH STANDARD. THIS DRAFT IS NOT CURRENT BEYOND 13 March 2009. This draft is issued to allow comments from interested parties; all comments will be given consideration prior to publication. No acknowledgement will normally be se

4、nt. See overleaf for information on commenting. No copying is allowed, in any form, without prior written permission from BSI except as permitted under the Copyright, Designs and Patent Act 1988 or for circulation within a nominating organization for briefing purposes. Electronic circulation is limi

5、ted to dissemination by e-mail within such an organization by committee members. Further copies of this draft may be purchased from BSI Customer Services, Tel: +44(0) 20 8996 9001 or email . British, International and foreign standards are also available from BSI Customer Services. Information on th

6、e co-operating organizations represented on the committees referenced above may be obtained from the responsible committee secretary. Cross-references The British Standards which implement International or European publications referred to in this draft may be found via the British Standards Online

7、Service on the BSI web site http:/. Direct tel: 020 8996 7009 Responsible Committee Secretary: Committee Service Centre (BSI) E-mail: Draft for Public Comment Head Office 389 Chiswick High Road London W4 4AL Telephone: +44(0)20 8996 9000 Fax: +44(0)20 8996 7001 Form 36 Version 8.0 DPC: 08/30182040

8、DC Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI b Introduction This draft standard is based on international discussions in which the UK has taken an active part. Your comments on this draft are invited and will assist in the prepar

9、ation of the consequent standard. Comments submitted will be reviewed by the relevant BSI committee before sending the consensus UK vote and comments to the international secretariat, which will then decide appropriate action on the draft and the comments received. If the international standard is a

10、pproved, it is possible the text will be published as an identical British Standard. UK Vote Please indicate whether you consider the UK should submit a negative (with reasons) or positive vote on this draft. Submission The guidance given below is intended to ensure that all comments receive efficie

11、nt and appropriate attention by the responsible BSI committee. Annotated drafts are not acceptable and will be rejected. All comments must be submitted, preferably electronically, to the Responsible Committee Secretary at the address given on the front cover. Comments should be compatible with Versi

12、on 6.0 or Version 97 of Microsoft Word for Windows, if possible; otherwise comments in ASCII text format are acceptable. Any comments not submitted electronically should still adhere to these format requirements. All comments submitted should be presented as given in the example below. Further infor

13、mation on submitting comments and how to obtain a blank electronic version of a comment form are available from the BSI web site at: http:/ Template for comments and secretariat observations Date: xx/xx/200x Document: ISO/DIS xxxxx 1 2 (3) 4 5 (6) (7) MB Clause No./ Subclause No./ Annex (e.g. 3.1) P

14、aragraph/ Figure/Table/ Note (e.g. Table 1) Type of com- ment Comment (justification for change) by the MB Proposed change by the MB Secretariat observations on each comment submitted 3.1 Definition 1 ed Definition is ambiguous and needs clarifying. Amend to read . so that the mains connector to whi

15、ch no connection . 6.4 Paragraph 2 te The use of the UV photometer as an alternative cannot be supported as serious problems have been encountered in its use in the UK. Delete reference to UV photometer. Microsoft and MS-DOS are registered trademarks, and Windows is a trademark of Microsoft Corporat

16、ion. Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM DRAFT prEN ISO 1211 November 2008 ICS 67.100.10Will supersede EN ISO 1211:2001 English Version Milk - Determination of fat content -

17、 Gravimetric method (Reference method) (ISO/DIS 1211:2008) Lait - Dtermination de la teneur en matire grasse - Mthode gravimtrique (Mthode de rfrence) (ISO/DIS 1211:2008) Milch - Bestimmung des Fettgehaltes - Gravimetrisches Verfahren (Referenzverfahren) (ISO/DIS 1211:2008) This draft European Stand

18、ard is submitted to CEN members for parallel enquiry. It has been drawn up by the Technical Committee CEN/TC 302. If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the

19、status of a national standard without any alteration. This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN M

20、anagement Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands,

21、 Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to provide supporting documentation. Warning : This docum

22、ent is not a European Standard. It is distributed for review and comments. It is subject to change without notice and shall not be referred to as a European Standard. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassa

23、rt, 36 B-1050 Brussels 2008 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. prEN ISO 1211:2008: E Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI prEN ISO 1211:2008 (E) 2

24、 Contents Page Foreword 3? Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI prEN ISO 1211:2008 (E) 3 Foreword This document (prEN ISO 1211:2008) has been prepared by Technical Committee ISO/TC 34 “Agricultural food products“ in collabor

25、ation with Technical Committee CEN/TC 302 “Milk and milk products - Methods of sampling and analysis” the secretariat of which is held by NEN. This document is currently submitted to the parallel Enquiry. This document will supersede EN ISO 1211:2001. Endorsement notice The text of ISO/DIS 1211:2008

26、 has been approved by CEN as a prEN ISO 1211:2008 without any modification. Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI THIS DOCUMENT IS A DRAFT CIRCULATED FOR COMMENT AND APPROVAL. IT IS THEREFORE SUBJECT TO CHANGE AND MAY NOT BE

27、REFERRED TO AS AN INTERNATIONAL STANDARD UNTIL PUBLISHED AS SUCH. IN ADDITION TO THEIR EVALUATION AS BEING ACCEPTABLE FOR INDUSTRIAL, TECHNOLOGICAL, COMMERCIAL AND USER PURPOSES, DRAFT INTERNATIONAL STANDARDS MAY ON OCCASION HAVE TO BE CONSIDERED IN THE LIGHT OF THEIR POTENTIAL TO BECOME STANDARDS T

28、O WHICH REFERENCE MAY BE MADE IN NATIONAL REGULATIONS. RECIPIENTS OF THIS DRAFT ARE INVITED TO SUBMIT, WITH THEIR COMMENTS, NOTIFICATION OF ANY RELEVANT PATENT RIGHTS OF WHICH THEY ARE AWARE AND TO PROVIDE SUPPORTING DOCUMENTATION. DRAFT INTERNATIONAL STANDARD ISO/DIS 1211 DRAFT INTERNATIONAL STANDA

29、RD ISO/IDF 1 International Organization for Standardization and International Dairy Federation, 2008 INTERNATIONAL ORGANIZATION FOR STANDARDIZATION ORGANISATION INTERNATIONALE DE NORMALISATION ISO/TC 34/SC 5 Voting begins on: 2008-11-27 Secretariat: NEN Voting terminates on: 2009-04-27 Milk Determin

30、ation of fat content Gravimetric method (Reference method) Lait Dtermination de la teneur en matire grasse Mthode gravimtrique (Mthode de rfrence) Revision of second edition (ISO 1211:1999) ICS 67.100.10 ISO/CEN PARALLEL ENQUIRY The CEN Secretary-General has advised the ISO Secretary-General that th

31、is ISO/DIS covers a subject of interest to European standardization. In accordance with the ISO-lead mode of collaboration as defined in the Vienna Agreement, consultation on this ISO/DIS has the same effect for CEN members as would a CEN enquiry on a draft European Standard. Should this draft be ac

32、cepted, a final draft, established on the basis of comments received, will be submitted to a parallel two-month FDIS vote in ISO and formal vote in CEN. In accordance with the provisions of Council Resolution 15/1993 this document is circulated in the English language only. Conformment aux dispositi

33、ons de la Rsolution du Conseil 15/1993, ce document est distribu en version anglaise seulement. This draft is submitted to a parallel enquiry vote in ISO and IDF. To expedite distribution, this document is circulated as received from the committee secretariat. ISO Central Secretariat work of editing

34、 and text composition will be undertaken at publication stage. Pour acclrer la distribution, le prsent document est distribu tel quil est parvenu du secrtariat du comit. Le travail de rdaction et de composition de texte sera effectu au Secrtariat central de lISO au stade de publication. Licensed Cop

35、y: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy, (c) BSI ISO/DIS 1211|IDF 1 ii ISO and IDF 2008 All rights reserved PDF disclaimer This PDF file may contain embedded typefaces. In accordance with Adobes licensing policy, this file may be printed or viewed

36、but shall not be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this file, parties accept therein the responsibility of not infringing Adobes licensing policy. The ISO Central Secretariat accepts no liability in thi

37、s area. Adobe is a trademark of Adobe Systems Incorporated. Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters were optimized for printing. Every care has been taken to ensure that the file is suitable for

38、use by ISO member bodies. In the unlikely event that a problem relating to it is found, please inform the Central Secretariat at the address given below. Copyright notice This ISO|IDF document is a Draft International Standard and is copyright-protected by ISO and IDF. Except as permitted under the

39、applicable laws of the users country, neither this ISO|IDF draft nor any extract from it may be reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic, photocopying, recording or otherwise, without prior written permission being secured. Requests for permissi

40、on to reproduce should be addressed to ISO or IDF at the respective address below. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org International Dairy Federation Diamant Building Bd Auguste Reyers 80 B-1030 B

41、russels Tel. + 32 2 733 98 88 Fax + 32 2 733 04 13 E-mail infofil-idf.org Web www.fil-idf.org Reproduction may be subject to royalty payments or a licensing agreement. Violators may be prosecuted. Licensed Copy: London South Bank University, South Bank University, 02/02/2009 04:04, Uncontrolled Copy

42、, (c) BSI ISO/DIS 1211 | IDF 1 ISO 2008 All rights reserved iii Contents 1 Scope1 2 Normative reference1 3 Terms and definitions.1 4 Principle .1 5 Reagents 2 6 Apparatus.2 7 Sampling 3 8 Preparation of test sample .4 9 Procedure.4 9.1 Test portion4 9.2 Blank tests .4 9.3 Preparation of fat-collecti

43、ng vessel.5 9.4 Determination 5 10 Calculation and expression of results 7 10.1 Calculation.7 10.2 Expression of results7 11 Precision 7 11.1 Interlaboratory test8 11.2 Repeatability8 11.3 Reproducibility 8 12 Test report8 Annex A (informative) Notes on procedures9 Annex B (informative) Alternative

44、procedure using fat-extraction tubes with siphon or wash-bottle fittings.11 Annex C (informative) Interlaboratory study on raw cow milk.14 Annex D (informative) Interlaboratory study on raw sheep milk and raw goat milk16 Licensed Copy: London South Bank University, South Bank University, 02/02/2009

45、04:04, Uncontrolled Copy, (c) BSI ISO/DIS 1211 | IDF 1 iv ISO 2008 All rights reserved Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out t

46、hrough ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO colla

47、borates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3. The main task of technical committees is to prepare International Sta

48、ndards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements o

49、f this International Standard may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 1211 | IDF 1 was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee SC 5, Milk and milk products and the International Dairy Federation (IDF). It is being published jointly

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