《BS-EN-13399-2003 BS-2000-517-2003.pdf》由会员分享，可在线阅读，更多相关《BS-EN-13399-2003 BS-2000-517-2003.pdf（10页珍藏版）》请在三一文库上搜索。
1、BRITISH STANDARD BS EN 13399:2003 BS 2000-517:2003 Methods of test for petroleum and its products BS 2000-517: Bitumen and bituminous binders Determination of storage stability of modified bitumen (Identical with IP 517-2004) The European Standard EN 13399:2003 has the status of a British Standard I
2、CS 75.140 ? Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN 13399:2003 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 16 January 2004 BSI 16 January 2004 ISBN 0 580 43272 6 Nat
3、ional foreword This British Standard is the official English language version of EN 13399:2003. The UK participation in its preparation was entrusted to Technical Committee PTI/13, Petroleum testing and terminology, which has the responsibility to: A list of organizations represented on this committ
4、ee can be obtained on request to its secretary. Energy Institute, under the brand of Institute of Petroleum publishes and sells all parts of BS 2000, and all BS EN petroleum test methods that would be part of BS 2000, both in its annual publication “Standard methods for analysis and testing of petro
5、leum and related products and British Standard 2000 parts” and individually. Further information is available from: Energy Institute, 61 New Cavendish Street, London W1G 7AR. Tel: 020 7467 7100. Fax: 020 7255 1472. Cross-references The British Standards which implement international or European publ
6、ications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the ne
7、cessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the in
8、terpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 6, an inside back cover and a
9、 back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME E
10、UROPENNE EUROPISCHE NORM EN 13399 December 2003 ICS 75.140 English version Bitumen and bituminous binders - Determination of storage stability of modified bitumen Bitumes et liants bitumineux - Dtermination de la stabilit au stockage des bitumes modifis Bitumen und bitumenhaltige Bindemittel - Besti
11、mmung der Lagerbestndigkeit von modifiziertem Bitumen This European Standard was approved by CEN on 21 November 2003. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without a
12、ny alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by
13、translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Icelan
14、d, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2003 CENAll rights
15、 of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 13399:2003 E Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13399:2003 (E) 2 Contentspage Foreword3 1Scope 3 2Normative references 3 3
16、Principle3 4Apparatus .4 4.1Tube.4 4.2Oven4 4.3Tins4 5Procedure .4 5.1General4 5.2Filling of the tube.4 5.3Closing of the tube 4 5.4Test conditions 4 5.5Recovery of the sample.4 6Test report 5 Bibliography6 Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled
17、Copy, (c) BSI EN 13399:2003 (E) 3 Foreword This document EN 13399:2003 has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical t
18、ext or by endorsement, at the latest by June 2004, and conflicting national standards shall be withdrawn at the latest by June 2004. This document includes a Bibliography. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to
19、implement this European Standard : Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and the United Kingdom. 1 Scope This European Standard specifies a
20、method for measuring the storage stability at high temperatures. NOTEModified bitumen and, in particular, polymer-modified bitumen, which consist of mainly bitumen and at least one additional agent, are known to display phase separation under certain conditions. WARNING The use of this European Stan
21、dard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the
22、 applicability of regulatory limitations prior to use. 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text, and the publications are listed hereafter.
23、For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to applies (including amendments). EN 581), Bitumen an
24、d bituminous binders Sampling bituminous binders. EN 12594, Bitumen and bituminous binders Preparation of test samples. 3 Principle A homogeneous sample of modified bitumen is maintained in a vertical vessel at 180 C or at a temperature specified by the producer for 3 days. After the sample has cool
25、ed down, it is cut into three equal parts. The two ends (top and bottom) are analysed further to evaluate possible differences in characteristics. If the chosen temperature differs from 180C, it shall be mentioned in the test report. 1)In course of revision Licensed Copy: sheffieldun sheffieldun, na
26、, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13399:2003 (E) 4 4 Apparatus Usual laboratory apparatus and glassware, together with the following: 4.1 Tube, of thin unvarnished aluminium, of height 160 mm minimum and of diameter 30 mm to 40 mm, closed at one end and typically “t
27、oothpaste tube“. 4.2 Oven, maintained at a temperature of 180 C 5 C for three consecutive days. 4.3 Tins, one to be marked “top“ and one to be marked “bottom“ (see 5.5), each of sufficient capacity to contain the combined upper and lower parts of different tubes. 5 Procedure 5.1 General Ensure that
28、the laboratory sample is representative of the modified bitumen to be analysed, in accordance with EN 58. Ensure that the laboratory sample is homogeneous and non-contaminated. Remove at least 150 g of the laboratory sample in accordance to EN 12594 and place it in a suitable container. 5.2 Filling
29、of the tube Heat the sample according to EN 12594 and re-homogenize using a stirrer. Pour the homogeneous liquid sample into the tube to a height of 100 mm to 120 mm, taking care to avoid incorporation of air bubbles. 5.3 Closing of the tube Ensure that the tube is tightly closed to avoid any action
30、 of air during high-temperature storage. A possibility for thermal expansion of the test material is necessary, and is created by squeezing the tube jacket slightly flat. After pouring the test material into the tube, and before the test material has completely cooled, press the open end of the tube
31、 together at a short distance below the test material surface. Ensure that no air remains by squeezing part of the test material from the tube. Press the end of the tube flat and fold the tube tightly several times. 5.4 Test conditions Within 1 h after filling, place the tube in the preheated oven i
32、n a vertical position. Ensure that the tube is maintained in a vertical position with an accuracy of 5 C at the chosen temperature for 72 h 1 h. 5.5 Recovery of the sample Remove the tube from the oven and let it cool down to room temperature, still in the same vertical position. Peel the aluminium
33、tube to recover the modified bitumen sample. NOTE 1For this operation it is recommended that the tube is placed in a refrigerating chamber, e.g. for 30 min at -20 C, and that the aluminium foil is then quickly removed. Place the recovered cylindrical sample horizontally on a clean flat surface and c
34、ut it into three equal parts with a heated knife. Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13399:2003 (E) 5 Place the top and bottom parts separately in the respective tins marked “top“ and “bottom“. NOTE 2The middle part is of no
35、use and should be eliminated. NOTE 3For characterisation tests (e.g softening point EN 1427 1; needle penetration, EN 1426 2 and others) it can be necessary to use more than one tube. In such cases, two or more tubes of the same sample should be tested simultaneously. 6 Test report The test report s
36、hall contain at least the following information: a) the type and identification of the sample under test; b) a reference to this European Standard; c) the measured values for the top and the bottom part according to the utilised European standards; d) any deviation, by agreement or otherwise, from t
37、he procedure specified; e) the date of the test. Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13399:2003 (E) 6 Bibliography 1 EN 1427, Bitumen and bituminous binders - Determination of softening point - Ring and Ball method. 2 EN 1426,
38、 Bitumen and bituminous binders Determination of needle penetration. Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI blank Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS 2000 Ser
39、ies The Institute of Petroleum 61. New Cavendish Street London W1G 7AR Tel:+44 (0)20 7467 7100 Fax:+44 (0)20 7255 1472 www.petroleum.co.uk Buying Parts of BS 2000 Orders for BS 2000 publications should be addressed to: The Library at the Institute of Petroleum British Standards Institution Customer
40、services 389 Chiswick High Road London W4 4AL Tel:+44 (0)20 8996 9001 Fax:+44 (0)20 8996 7001 www.bsi- Order hard copy standards securely via: www.bsi- Copyright Copyright subsists in all BS 2000 publications. No part of this publication may be reproduced in any form without the prior permission in writing of BSI and the IP. Enquiries about copyright should be made to the Secretary of PTI/13 at the IP. PTI/13 Licensed Copy: sheffieldun sheffieldun, na, Mon Oct 30 05:07:57 GMT+00:00 2006, Uncontrolled Copy, (c) BSI