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1、BRITISH STANDARD BS EN ISO 105-E13:1997 Textiles Tests for colour fastness Part E13: Colour fastness to acid-felting: Severe The European Standard EN ISO 105-E13:1996 has the status of a British Standard ICS 59.080.01 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Un
2、controlled Copy, (c) BSI BS EN ISO 105-E13:1997 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 April 1997 BSI 11-1998 The following BSI references re
3、late to the work on this standard: Committee reference TCI/25 Special announcement in BSI News June 1996 ISBN 0 580 27308 3 Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee TCI/25, Chemical properties, upon which the follo
4、wing bodies were represented: Association of Consulting Scientists Association of Suppliers to the British Clothing Industry British Apparel and Textile Confederation British Clothing Industry Association British Measurement and Testing Association Chemical Industries Association Consumer Policy Com
5、mittee of BSI Fabric Care Research Association Ltd. Home Laundering Consultative Council International Wool Secretariat Mail Order Traders Association Ministry of Defence National Wool Textile Export Corporation SATRA Footwear Technology Centre Soap and Detergent Industry Association Society of Dyer
6、s and Colourists Textile Finishers Association Participation in the detailed technical work was undertaken by the Society of Dyers and Colourists Amendments issued since publication Amd. No.DateComments Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy
7、, (c) BSI BS EN ISO 105-E13:1997 BSI 11-1998i Contents Page Committees responsibleInside front cover National forewordii Foreword2 Forewordiii Text of EN ISO 105-E131 List of referencesInside back cover Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy
8、, (c) BSI BS EN ISO 105-E13:1997 ii BSI 11-1998 National foreword This British Standard has been prepared by Technical Committee TCI/25, and is the English language version of EN ISO 105-E13:1996 Textiles Tests for colour fastness Part E13: Colour fastness to acid-felting: Severe published by the Eu
9、ropean Committee for Standardization (CEN). It is identical with ISO 105-E13:1994, published by the International Organization for Standardization (ISO). This British Standard supersedes the corresponding method in BS 1006:1990, which is withdrawn by amendment. A British Standard does not purport to
10、 include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application Compliance with a British Standard does not of itself confer immunity from legal obligations. Cross-references Publication referred toCorresponding British Standard BS EN ISO
11、 105 Textiles Tests for colour fastness EN ISO 105-A01:1995Part A01:1996 General principles of testing BS EN 20105 Textiles Tests for colour fastness EN 20105-A02:1994Part A02:1995 Grey scale for assessing change in colour EN 20105-A03:1994Part A03:1995 Grey scale for assessing staining EN ISO 105-F
12、:1985BS 1006:1990 Methods of test for colour fastness of textiles and leather Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, the EN ISO title page, page 2, the ISO title page, pages ii to iv, pages 1 to 4, an inside back cover and a back cover. This st
13、andard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE
14、 EUROPISCHE NORM EN ISO 105-E13 December 1996 ICS 59.080.10 Descriptors: See ISO document English version Textiles Tests for colour fastness Part E13: Colour fastness to acid-felting: Severe (ISO 105-E13:1994) Textiles Essais de solidit des teintures Partie E13: Solidit des teintures au foulon acide
15、: Essai fort (ISO 105-E13:1994) Textilien Farbechtheitsprfungen Teil E13: Farbechtheit gegen saures Walken: schwere Beanspruchung (ISO 105-E13:1994) This European Standard was approved by CEN on 1996-11-30. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the
16、 conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. The European Standards exist in t
17、hree official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own Language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of
18、Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat
19、: rue de Stassart 36, B-1050 Brussels 1996 Copyright reserved to CEN members Ref. No. EN ISO 105-E13:1996 E Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E13:1996 BSI 11-1998 2 Foreword The text of the International Standard fro
20、m Technical Committee ISO/TC 38 “Textiles” of the International Organization for Standardization (ISO) has been taken over as an European Standard by Technical Committee CEN/TC 248 “Textile and textile products”, the secretariat of which is held by BSI. This European Standard shall be given the stat
21、us of a national standard, either by publication of an identical text or by endorsement, at the latest by June 1997, and conflicting national standards shall be withdrawn at the latest by June 1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the follow
22、ing countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard I
23、SO 105-E13:1994 has been approved by CEN as a European Standard without any modification. NOTENormative references to International Standards are listed in annex ZA (normative). Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Licensed Copy:
24、sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E13:1996 ii BSI 11-1998 Contents Page Forewordiii 1Scope1 2Normative references1 3Principle1 4Apparatus and reagents1 5Test specimen1 6Procedure1 7Test report2 Annex ZA (normative)3 Licensed Copy:
25、sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E13:1996 BSI 11-1998iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing Internati
26、onal Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with IS
27、O, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an Int
28、ernational Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard ISO 105-E13 was prepared by Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. This third edition cancels and replaces the second edi
29、tion (ISO 105-E13:1987), of which it constitutes a technical revision. ISO 105 was previously published in thirteen “parts”, each designated by a letter (e.g. “Part A”), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part l
30、etter and by a two-digit serial number (e.g. “Section A01”). These sections are now being republished as separate documents, themselves designated “parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. Descriptors: Textiles, dyes, tests
31、, chemical tests, acid resistance tests, determination, colour fastness. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI iv blank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN I
32、SO 105-E13:1996 BSI 11-19981 1 Scope This part of ISO 105 specifies a method for determining the resistance of the colour of textiles of all forms to the action of acids, as used under severe conditions in the acid-felting process. 2 Normative references The following standards contain provisions wh
33、ich, through reference in this text, constitute provisions of this part of ISO 105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of applying
34、the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1994, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02
35、: Grey scale for assessing change in colour. ISO 105-A03:1993, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Textiles Tests for colour fastness Part F: Standard adjacent fabrics. 3 Principle A specimen of the textile in contact with adjacent fabrics
36、is milled in solutions of acetic acid and/or sulfuric acid, rinsed and dried. The change in colour of the specimen and the staining of the adjacent fabrics are assessed by comparison with the grey scales. 4 Apparatus and reagents 4.1 Suitable open container and glass rod, flattened at one end, or ap
37、propriate mechanical device (see 6.2). 4.2 Sulfuric acid, aqueous solution containing 1 ml of concentrated sulfuric acid (A 1,84 g/ml) per litre. 4.3 Acetic acid, aqueous solution containing 5 ml of acetic acid (300 g/ml) per litre. 4.4 Two adjacent fabrics, in accordance with the appropriate sectio
38、n F01 to F08 of ISO 105-F:1985, each measuring 40 mm 100 mm, one piece made of wool and the other made of wool or of another fibre, as desired, to be assessed for staining. 4.5 Grey scale for assessing change in colour, complying with ISO 105-A02, and grey scale for assessing staining, complying wit
39、h ISO 105-A03. 5 Test specimen 5.1 If the textile to be tested is fabric, attach a specimen measuring 40 mm 100 mm between the two adjacent fabrics (4.4), also measuring 40 mm 100 mm, by sewing along one of the shorter sides. 5.2 If the textile to be tested is yarn, knit it into fabric and treat it
40、as in 5.1, or form a layer of parallel lengths of it between the two adjacent fabrics (4.4), the amount of yarn taken being approximately equal to half the combined mass of the adjacent fabrics. Sew along all four sides to hold the yarn in place and to form a composite specimen. 5.3 If the textile t
41、o be tested is loose fibre, comb and compress an amount approximately equal to half the combined mass of the adjacent fabrics (4.4) into a sheet 40 mm 100 min. Place the sheet between the two adjacent fabrics and sew along all four sides to hold the fibres in place and to form a composite specimen.
42、6 Procedure 6.1 Test the composite specimen in accordance with 6.2 to 6.4 inclusive, using sulfuric acid solution (4.2) and acetic acid solution (4.3) in separate tests, or using only one of these reagents, as required. The liquor ratio in both cases shall be 40 : 1. 6.2 If possible, use a mechanica
43、l milling device set to give results identical with those obtained in a manual milling test. NOTE 1Other mechanical devices may be used for the test provided that equivalent results are obtained. 6.3 Bring the test solution to 90 C 2 C in the container, and immerse the composite specimen in the solu
44、tion for 30 min, maintaining this temperature. 6.4 When milling by hand, move the composite specimen about continuously with the glass rod while it is in the milling-bath, and press it with the rod every 2 min, without removing it from the bath. 6.5 Rinse the milled composite specimen for 10 min in
45、cold, running tap-water and drain it. Open out the composite specimen (by breaking the stitching on all sides except one of the shorter sides if necessary) and dry it by hanging it in air at a temperature not exceeding 60 C, with the parts in contact only at the line of stitching. 6.6 Assess the cha
46、nge in colour of the specimen and the staining of the adjacent fabrics by comparison with the grey scales (4.5). Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E13:1996 2 BSI 11-1998 7 Test report The test report shall include th
47、e following information: a) the number and year of publication of this part of ISO 105, i.e. ISO 105-E13:1994; b) all details necessary for the identification of the sample tested; c) for each reagent used, the numerical grey scale rating for change in colour of the test specimen; d) for each reagen
48、t used, the numerical grey scale rating for staining of the adjacent fabrics, and the type of adjacent fabric used. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:08 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E13:1996 BSI 11-19983 Annex ZA (normative) Normative references to
49、 international publications with their relevant European publications This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the p