BS-EN-ISO-2815-2003 BS-3900-E9-2003.pdf

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1、BRITISH STANDARD BS EN ISO 2815:2003 BS 3900-E9:2003 Paints and varnishes Buchholz indentation test The European Standard EN ISO 2815:2003 has the status of a British Standard ICS 87.040 ? BS EN ISO 2815:2003 This British Standard was published under the authority of the Standards Policy and Strateg

2、y Committee on 20 August 2003 BSI 20 August 2003 ISBN 0 580 42485 5 National foreword This British Standard is the official English language version of EN ISO 2815:2003. It is identical with ISO 2815:2003. It supersedes BS EN ISO 2815:1998 which is withdrawn. The UK participation in its preparation

3、was entrusted to Technical Committee STI/10, Test methods for paints, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications refe

4、rred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provi

5、sions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation,

6、 or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pag

7、es ii to iv, pages 1 to 10, the Annex ZA page and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 2815 April 2003 ICS 87.0

8、40Supersedes EN ISO 2815:1998 English version Paints and varnishes - Buchholz indentation test (ISO 2815:2003) Peintures et vernis - Essais dindentation Buchholz (ISO 2815:2003) Beschichtungsstoffe - Eindruckversuch nach Buchholz (ISO 2815:2003) This European Standard was approved by CEN on 25 March

9、 2003. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtain

10、ed on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centr

11、e has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and U

12、nited Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2003 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 2815

13、:2003 E I NESO 82:5102( 30E) 2 CORRECTED 2003-07-16 Foreword This document (EN ISO 2815:2003) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes“ in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes“, the secretariat of which is held by DIN. This European

14、Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 2003, and conflicting national standards shall be withdrawn at the latest by October 2003. This document supersedes EN ISO 2815:1998. According to the CEN

15、/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portuga

16、l, Slovakia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 2815:2003 has been approved by CEN as EN ISO 2815:2003 without any modifications. NOTE Normative references to International Standards are listed in Annex ZA (normative). EN ISO 2815:2003 Reference num

17、ber ISO 2815:2003(E) OSI 3002 INTERNATIONAL STANDARD ISO 2815 Second edition 2003-04-01 Paints and varnishes Buchholz indentation test Peintures et vernis Essais dindentation Buchholz EN ISO 2815:2003 IS:5182 O3002(E) DPlcsid Fremia ihTs PDF file mya ctnoian emdebt dedyfepcaes. In ccacnadrow eitA he

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22、. 4 + 10 947 22 1 11 xaF0 947 22 14 + 9 74 E-mial coirypthgis.o gro We bwww.is.o gro ii ISO 3002 Allr ihgtsser edevr EN ISO 2815:2003 IS:5182 O3002(E) I SO 3002 All irhgts seredevr iii Contents Page Forewordiv 1 Scope1 2 Normative references .1 3 Principle.1 4 Apparatus.1 5 Sampling4 6 Test panels 4

23、 7 Procedure.5 8 Calculation and expression of results6 9 Precision6 10 Test report7 Annex A (informative) Buchholz indentation resistance8 EN ISO 2815:2003 IS:5182 O3002(E) iv I SO 3002 All irhgts seredevr Foreword ISO (the International Organization for Standardization) is a worldwide federation o

24、f national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. In

25、ternational organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with

26、the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval

27、 by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 2815 was prepared by Technical Committee I

28、SO/TC 35, Paints and varnishes, Subcommittee SC 9, General test methods for paints and varnishes. This second edition cancels and replaces the first edition (ISO 2815:1973), which has been technically revised. The main changes are as follows: only indentation length is now determined; the conversion

29、 of indentation length to indentation resistance is described in an informative annex. EN ISO 2815:2003 INTENRATIONAL TSANDADR IS:5182 O3002(E) I SO 3002 All irhgts seredevr 1 Paints and varnishes Buchholz indentation test 1 Scope This International Standard describes a method for carrying out an in

30、dentation test on a single coating or multicoat system of paint, varnish or related product, using a Buchholz indentor. The length of the indentation produced is indicative of the residual deformation of the coating. This indentation test is not suitable for products which contain a strong plasticiz

31、er. NOTE 1 Since the indentation test, like other physical tests on paints, gives results which can be dependent upon time, temperature and humidity, comparable results will only be obtained if the test is carried out under well-defined conditions. NOTE 2 Since the indentation depth depends upon the

32、 film thickness, the result obtained for the indentation length is only valid if the coating thickness exceeds a certain minimum value (see Annex A). 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the editi

33、on cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 1513, Paints and varnishes Examination and preparation of samples for testing ISO 1514, Paints and varnishes Standard panels for testing ISO 2808, Paints and varnishes Dete

34、rmination of film thickness ISO 15528, Paints, varnishes and raw materials for paints and varnishes Sampling 3 Principle An indentor of specified size and shape is applied to the coating under defined conditions. The indentation length is measured in millimetres (see Annex A). 4 Apparatus 4.1 Indent

35、ation apparatus This is shown in Figure 1. It consists essentially of a rectangular block of metal, which forms the body of the instrument, an indentor and two pointed feet. EN ISO 2815:2003 IS:5182 O3002(E) 2 I SO 3002 All irhgts seredevr Figure 1 Indentation apparatus (oblique underside view) The

36、indentor is a sharpened sharp-edged metal wheel of hardened tool steel. The cross-section through its axis of rotation and its dimensions shall be as shown in Figure 2. Figures 3a) and 3b) show the shape of the indentation produced. Dimensions in millimetres Key 1 sharp edge 2 indentor 3 coating 4 s

37、ubstrate Figure 2 Buchholz indentor EN ISO 2815:2003 IS:5182 O3002(E) I SO 3002 All irhgts seredevr 3 a) Shape of indentation b) Indentation length l (mm) and indentation depth h (m) (enlarged) Key 1 coating Figure 3 Shape of indentation The indentor and the two feet are so positioned in the body th

38、at, when the instrument is placed on a level surface, it is stable, its upper surface is horizontal and the effective load upon the indentor is (500 5) g. 4.2 Measuring device A suitable device for measuring the length of the indentation consists of a microscope with 20 magnification and an eyepiece

39、 fitted with a graduated scale capable of reading to 0,1 mm. The area of indentation shall be illuminated by means of a light source located so that the angle of incidence of the light exceeds 60, as shown in Figure 4. The microscope shall be positioned vertically over the illuminated area and focus

40、ed to bring the shadow produced by the indentation (see Figures 4 and 5) and the graduated scale together. NOTE The position of the indentation mark can be located by means of a suitable template prepared from a triangular sheet of transparent plastics film (see Figure 6). Key 1 light source 2 micro

41、scope 3 indentation 4 coating 5 substrate Figure 4 Position of the light source and the microscope EN ISO 2815:2003 IS:5182 O3002(E) 4 I SO 3002 All irhgts seredevr Key 1 indentation visible by its shadow 2 light source Figure 5 Shadow produced by the indentation Key 1 position of the indentation 2

42、position of the feet of the instrument Figure 6 Template to locate the position of the indentation 4.3 Timing device Use a stopwatch or other suitable timing device capable of measuring 30 s to the nearest 1 s. 5 Sampling Take a representative sample of the product to be tested (or of each product i

43、n the case of a multicoat system), as described in ISO 15528. The sample shall then be examined and prepared for testing as described in ISO 1513. 6 Test panels 6.1 Materials and dimensions Unless otherwise agreed, the test panels shall be of metal or glass conforming to the requirements of ISO 1514

44、. The test panels shall be flat and free from distortion, and the surface shall be free from any visible ridges or cracks. EN ISO 2815:2003 IS:5182 O3002(E) I SO 3002 All irhgts seredevr 5 Unless otherwise agreed, the test panels shall have minimum dimensions of 150 mm 100 mm and a thickness of not

45、less than 0,75 mm. NOTE The test panels may be cut to size after coating and drying, provided no distortion occurs. 6.2 Preparation and coating of panels The test panels shall be prepared in accordance with ISO 1514, unless otherwise agreed, and shall then be coated by the specified method with the

46、product or system under test to the specified film thickness limits. Any variation from the requirements of ISO 1514 shall be noted in the test report (see Clause 10). 6.3 Drying and conditioning of the test panels The coated test panels shall be dried (or stoved) and aged (if applicable) for the sp

47、ecified time and under the specified conditions and, unless otherwise specified, shall be conditioned at a temperature of (23 2) C and a relative humidity of (50 5) % for a minimum of 16 h. The test procedure shall then be carried out as soon as possible. 6.4 Thickness of coating The average thickne

48、ss, in micrometres, of the dry coating in the region to be tested shall be determined by the method specified, using one of the procedures specified in ISO 2808. 7 Procedure 7.1 Ambient conditions The test shall be carried out at a temperature of (23 2) C and a relative humidity of (50 5) %, unless

49、otherwise agreed. 7.2 Determination of indentation length Place the test panel, paint film uppermost, on a firm horizontal surface. Take the indentation apparatus (4.1) and place it gently and without any tilting or lateral movement on the test panel, leave the indentor in position for (30 1) s and remove it carefully. When the apparatus is put in place, the feet of the apparatus shall first

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