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1、BRITISH STANDARD BS EN ISO 105-X13:1997 Textiles Tests for colour fastness Part X13: Colour fastness of wool dyes to processes using chemical means for creasing, pleating and setting (ISO 105-X13:1994) The European Standard EN ISO 105-X13:1997 has the status of a British Standard ICS 59.080.01 Licen
2、sed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 105-X13:1997 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and c
3、omes into effect on 15 August 1997 BSI 09-1999 ISBN 0 580 27878 6 National foreword This British Standard is the English language version of EN ISO 105-X13:1997. It is identical with ISO 105-X13:1994. It supersedes the relevant method in BS 1006:1990 which is withdrawn by amendment. The UK participa
4、tion in its preparation was entrusted by Technical Committee TCI/25, Chemical properties, to Subcommittee TCI/25/-/10, Colour fastness, which has the responsibility to: aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretati
5、on, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references Attention is drawn to the fac
6、t that Annex ZA lists normative references to international publications with their corresponding European publications. The British Standards which implement these international or European publications may be found in the BSI Standards Catalogue under the section entitled “International Standards
7、Correspondence Index”, or using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does
8、not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, the EN ISO title page, page 2, the ISO title page, pages ii to iv, pages 1 to 4 and a back cover. This standard has been updated (see copyright date) a
9、nd may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Amendments issued since publication Amd. No.DateComments Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 105-X13:1997
10、 BSI 09-1999i Contents Page National forewordInside front cover Foreword2 Forewordiii Text of ISO 105-X131 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ii blank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 200
11、6, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-X13 April 1997 ICS 59.080.01 Descriptors: See ISO document English version Textiles Tests for colour fastness Part X13: Colour fastness of wool dyes to processes using chemical means for creasing, pleating and
12、 setting (ISO 105-X13:1994) Textiles Essais de solidit des teintures Partie X13: Solidit des teintures sur laine aux traitements effectus avec des produits chimiques en vue du plissage et du fixage (ISO 105-X13:1994) Textilien Farbechtheitsprfungen Teil X13: Farbechtheit von Wollfarbstoffen gegen Pr
13、ozesse zum Falten, Plissieren und Fixieren auf chemischem Wege (ISO 105-X13:1994) This European Standard was approved by CEN on 1997-03-28. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a natio
14、nal standard without any alteration. Up-to-date Lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. The European Standards exist in three official versions (English, French, German). A version in any
15、other language made by translation under the responsibility of a CEN member into its own Language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Icelan
16、d, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1997 CEN ALL rights of exploi
17、tation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 105-X13:1997 E Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X13:1997 BSI 09-1999 2 Foreword The text of the International Standard
18、 from Technical Committee ISO/TC 38 “Textiles” of the International Organization for Standardization (ISO) has been taken over as an European Standard by Technical Committee CEN/TC 248 “Textiles and textile products”, the secretariat of which is held by BSI. This European Standard shall be given the
19、 status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 1997, and conflicting national standards shall be withdrawn at the latest by October 1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of
20、 the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International
21、 Standard ISO 105-X13:1994 has been approved by CEN as a European Standard without any modification. NOTENormative references to International Standards are listed in Annex ZA (normative). Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Lice
22、nsed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X13:1997 ii BSI 09-1999 Contents Page Forewordiii 1Scope1 2Normative references1 3Principle1 4Apparatus and reagent1 5Test specimens1 6Procedure2 7Test report2 Annex ZA (normative) Norma
23、tive references to international publications with their relevant European publications4 Figure 1 Composite specimen3 Descriptors: Textiles, wool, dyes, tests, chemical tests, determination, colour fastness. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled
24、 Copy, (c) BSI EN ISO 105-X13:1997 BSI 09-1999iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each
25、 member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the Internationa
26、l Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies c
27、asting a vote. International Standard ISO 105-X13 was prepared by Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. This fourth edition cancels and replaces the third edition (ISO 105-X13:1987), of which it constitutes a technical revision. ISO 10
28、5 was previously published in thirteen “parts”, each designated by a letter (e.g. “Part A”), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (e.g. “Section A01”). These sections a
29、re now being republished as separate documents, themselves designated “parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI iv b
30、lank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X13:1997 BSI 09-19991 1 Scope This part of ISO specifies a method for determining the resistance of the colour of wool textiles of all kinds to processes using chemical means in
31、 conjunction with steam for creasing, pleating and setting purposes. 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisions of this part of ISO 105. At the time of publication, the editions indicated were valid. All standards ar
32、e subject to revision, and parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1994,
33、Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. ISO 105-A03:1993, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Text
34、iles Tests for colour fastness Part F: Standard adjacent fabrics. 3 Principle A specimen of the textile, treated with the chemical solution, is placed in contact with specified adjacent fabrics and subjected to steam pressing. A comparison specimen, not treated with the chemical solution, is steam-p
35、ressed simultaneously. The specimens are dried and any differences between the colour of the two specimens and the staining of the adjacent fabrics are assessed by comparison with the grey scales. 4 Apparatus and reagent 4.1 Steam press, flat bed, with steam supply at a pressure of not less than 415
36、 kPa. The press should be at its normal operating temperature to avoid anomalous results due to condensation. When starting from cold, the press should be run six times through the standard cycle (see 6.5) without test specimens. 4.2 Apparatus capable of giving a fine, uniform spray, constructed fro
37、m chemically inert materials. 4.3 Chemical solution, at the recommended concentration. This test procedure was established with an aqueous solution containing a volume fraction of 5 % mono-ethanolamine sesquisulfite to which was added a 0,3 % volume fraction of any suitable wetting agent. The method
38、 may be adapted to the use of other chemical products, provided that allowance is made for any recommendations as to working concentration; 3 g of a wetting agent should be added per litre of solution, irrespective of its composition. 4.4 Glass plate, 100 mm 150 mm, on which the specimen is laid for
39、 spraying. 4.5 Eight single-fibre adjacent fabrics, complying with the relevant sections of F01 to F08 of ISO 105-F:1985, each measuring 80 mm 110 mm, four of wool and four normally of cotton. When staining of a fibre other than cotton is of greater interest, the cotton may be replaced by an alterna
40、tive material having a smooth finish and made of this fibre. 4.6 Backing material Some dyes can even stain the press covers. The use of a protective plain backing material is therefore specified; thick cotton fabric or paper towelling has been found satisfactory. 4.7 Grey scale for assessing change
41、in colour, complying with ISO 105-A02, and grey scale for assessing staining, complying with ISO 105-A03. 5 Test specimens 5.1 If the textile to be tested is fabric, use two specimens measuring 100 mm 150 mm identically oriented. 5.2 If the textile to be tested is yarn, either knit it into fabric an
42、d treat as in 5.1 or form a layer of parallel lengths of mass approximately half the combined mass of the four adjacent fabrics (4.5), two of each kind, in the composite specimen (see 5.3). If the textile to be tested is loose fibre, comb and compress an amount approximately equal to half the combin
43、ed mass of the adjacent fabrics into a sheet 100 mm 150 mm. 5.3 Place each specimen between four adjacent fabrics, one of each kind on each side, to form a composite specimen. Two composite specimens are required for each test, one to contain the treated specimen (see 5.3.1), the other to contain th
44、e comparison specimen (see 5.3.2). Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:22 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X13:1997 2 BSI 09-1999 5.3.1 Composite treated specimen. Cover one-half of each side of the treated specimen with the wool adjacent fabric, the clo
45、th on top of the specimen being prewetted (see 6.2). Cover the other half of each side with the cotton adjacent fabric or alternative material (see 4.5). The composite specimen shall be backed on each side (see 4.6). The composite specimen with backing is illustrated in Figure 1. 5.3.2 Composite com
46、parison specimen. This is identical with the composite treated specimen (5.3.1) except that the specimen is not treated and the upper wool adjacent fabric is not prewetted. 6 Procedure 6.1 Assemble the composite comparison specimen (5.3.2). 6.2 Wet out one only of the four wool adjacent fabrics for
47、1 min in boiling distilled water, hydroextract to approximately 50 % expression and store in a suitable container. The use of prewetted wool adjacent fabric, only on the sprayed surface of the specimen, gives more uniformity of any staining. The wool adjacent fabric in the composite comparison speci
48、men shall not be prewetted, since this specimen is intended to reproduce the effect of steam pressing only. It will be found convenient to wet out the number of wool adjacent fabrics required for a series of tests in the manner described in the preceding paragraph and to store these in a container s
49、uch as a polyethylene bag to maintain the water content. NOTE 1See ISO 105-A01:1994, subclause 11.4, concerning wetting out of wool specimens. 6.3 Weigh the remaining specimen, place it on the glass plate (4.4) with the surface to be assessed facing upwards and uniformly spray this surface with the chemical solution (4.3) to a mass increase of 100 %. 6.4 Assemble the composite treated specimen (5.3.1), sprayed surface up, with the wetted wool adjacent fabric on the sprayed surface. 6.5 Not more than 2 min after spraying,