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1、BRITISH STANDARD BS EN ISO 13503-3:2005 Incorporating corrigendum no. 1 Petroleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy brines The European Standard EN ISO 13503-3:2005 has the status of a British Standard ICS 75.100 ? Licensed Copy: London South Bank Un
2、iversity, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI BS EN ISO 13503-3:2005 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 13 January 2006 BSI 2007 ISBN 978 0 580 60342 6 National foreword Th
3、is British Standard is the UK implementation of EN ISO 13503-3:2005, incorporating corrigendum July 2007. It is identical with ISO 13503-3:2005, incorporating corrigendum April 2006. The UK participation in its preparation was entrusted by Technical Committee PSE/17, Material and equipment for petro
4、leum, petrochemical and natural gas industries, to Subcommittee PSE/17/-/3, Drilling and completion fluids and well cements. A list of organizations represented on this subcommittee can be obtained on request to its secretary. This publication does not purport to include all the necessary provisions
5、 of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publication Amd. No. DateComments 17385 Corrigendum No. 1 31 October 2007Correction to French title on the EN ISO cover page an
6、d ISO cover page Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13503-3 December 2005 ICS 75.100 English Version Petroleum and natural gas industries -
7、Completion fluids and materials - Part 3: Testing of heavy brines (ISO 13503-3:2005) Erdl- und Erdgasindustrie - Komplettierungsflssigkeiten und -materialien - Teil 3: Prfung von schweren Solen (ISO 13503-3:2005) This European Standard was approved by CEN on 9 December 2005. CEN members are bound to
8、 comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Centra
9、l Secretariat or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as th
10、e official versions. CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain
11、, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2005 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Me
12、mbers. Ref. No. EN ISO 13503-3:2005: E Industries du ptrole et du gaz naturel - Fluides de denses (ISO 13503-3:2005) matriaux compltion et - Partie 3: Essais de saumures Incorporating corrigendum July 2007 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50
13、 GMT+00:00 2007, Uncontrolled Copy, (c) BSI Foreword This document (EN ISO 13503-3:2005) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipmen
14、t and offshore structures for petroleum, petrochemical and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2006, and confli
15、cting national standards shall be withdrawn at the latest by June 2006. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finlan
16、d, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of ISO 13503-3:2005 has been approved by CEN as EN ISO 13503-3:200
17、5 without any modifications. EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI Reference number ISO 13503-3:2005(E) INTERNATIONAL STANDARD ISO 13503-3 First edition 2005-12-15 Petroleum and na
18、tural gas industries Completion fluids and materials Part 3: Testing of heavy brines Partie 3: Essais de saumures denses EN ISO 13503-3:2005 Industries du ptrole et du gaz naturel Fluides de matriaux et compltion Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 0
19、1:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI ii Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI iii Contents Page Foreword. v Introduction. vi 1 Scope . 1 2 Normative references. 1 3 Terms, definitions an
20、d abbreviated terms . 2 3.1 Terms and definitions. 2 3.2 Symbols and abbreviated terms . 2 4 Requirements 4 4.1 Quality control instructions. 4 4.2 Records retention. 4 5 Calibration of equipment . 4 5.1 General requirements. 4 5.2 Reagents and materials for calibration 4 5.3 General requirements fo
21、r calibration of particular apparatus . 5 5.4 Frequency of calibration verification 5 5.5 Calibration verification. 6 6 Density. 7 6.1 General. 7 6.2 Apparatus 9 6.3 Density measurement by hydrometer 10 6.4 Density correction to 21 C (70 F) 11 6.5 Calculation of density in units other than kg/m3. 13
22、 6.6 Calculation for pressure and temperature compensation 14 7 Crystallization temperature . 16 7.1 Principle. 16 7.2 Apparatus 20 7.3 Determination of crystallization point 21 7.4 Calculation of crystallization point. 21 8 Brine clarity. 22 8.1 Principle. 22 8.2 Apparatus 22 8.3 Determination of b
23、rine clarity 23 9 Solids evaluation by gravimetric procedures 23 9.1 Principle. 23 9.2 Apparatus 24 9.3 Preparation of glass-fibre filter disk. 24 9.4 Selection of sample volume 25 9.5 Determination of total suspended solids. 25 9.6 Calculation of total suspended solids 26 9.7 Calculation of precisi
24、on and bias . 26 9.8 Determination of volatile and non-volatile solids 26 9.9 Calculation of non-volatile and volatile solids 27 10 pH . 27 10.1 Principle. 27 10.2 Reagents and materials . 28 10.3 Apparatus 28 10.4 Measurement of pH. 29 EN ISO 13503-3:2005 Licensed Copy: London South Bank University
25、, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI iv 10.5 Precision statement30 10.6 Care of the electrode 30 11 Iron contamination30 11.1 Principle.30 11.2 Reagents and materials31 11.3 Apparatus.31 11.4 Preparation of colorimetric standards32 11.5 Measu
26、rement of iron contamination.32 11.6 Precision statement33 12 Daily completion fluid report .33 12.1 Principle.33 12.2 Well identification, geometry and zone data34 12.3 System properties.34 12.4 Fluids accounting .35 12.5 Cost accounting35 12.6 Daily commentary .35 12.7 Vendor representative identi
27、fication.35 Annex A (informative) Completion fluids report form.36 Annex B (informative) Gas hydrates.37 Annex C (informative) Buffering capacity of brines38 Annex D (informative) Pressure crystallization of brines.39 Annex E (informative) Brine viscosity40 Annex F (informative) Principle of corrosi
28、on testing41 Bibliography .43 EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI v Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standa
29、rds bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organ
30、izations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given i
31、n the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 %
32、 of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13503-3 was prepared by Technical Committee ISO/TC 67, Mate
33、rials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. ISO 13503 consists of the following parts, under the general title Petroleum and natural gas industries Completion fluids and materia
34、ls: Part 1: Measurement of viscous properties of completion fluids Part 3: Testing of heavy brines The following parts are under preparation: Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel packing operations Part 4: Procedure for measuring stimulation and grav
35、el-pack fluid leakoff under static conditions Part 5: Procedure for measuring the long-term conductivity of proppants EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI vi Introduction This par
36、t of ISO 13503 covers heavy brines commonly used in petroleum and natural gas completion, workover and drill-in fluids. These brines can be purchased or rented from multiple sources, and are available worldwide. No single source or limited source of supply is included, either by inference or referen
37、ce. Annexes A to F are given for information. EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI 1 Petroleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy
38、brines 1 Scope This part of ISO 13503 covers the physical properties, potential contaminants and test procedures for heavy brine fluids manufactured for use in oil and gas well drilling, completion and workover fluids. This part of ISO 13503 provides methods for assessing the performance and physica
39、l characteristics of heavy brines for use in field operations. It includes procedures for evaluating the density or specific gravity, the clarity or amount of particulate matter carried in the brine, the crystallization point or the temperature (both ambient and under pressure) at which the brines m
40、ake the transition between liquid and solid, the pH, and iron contamination. It also contains a discussion of gas hydrate formation and mitigation, brine viscosity, corrosion testing, buffering capacity and a standardised reporting form. This part of ISO 13503 is intended for the use of manufacturer
41、s, service companies and end-users of heavy brines. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including
42、 any amendments applies). ISO 10414-1:2001, Petroleum and natural gas industries Field testing of drilling fluids Part 1: Water-based fluids ASTM 1) E77, Standard Test Method for Inspection and Verification of Thermometers NIST 2) SRM 185h, Potassium Hydrogen Phthalate, pH Standard NIST SRM 186g, Po
43、tassium Dihydrogen Phosphate, pH Standard NIST SRM 191C, pH Standards NBS (NIST) Circular 555, Testing of Hydrometers, 22 Oct 1954 1) ASTM, American Society for Testing and Materials, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, USA. http:/www.astm.org. 2) NIST, National I
44、nstitute of Standards and Technology, 100 Bureau Drive, Stop 3460, Gaithersburg, MD 20899-3460, USA. http:/www.nist.gov. EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Uncontrolled Copy, (c) BSI 2 3 Terms, definition
45、s and abbreviated terms For the purposes of this document, the following terms, definitions and abbreviated terms apply. 3.1 Terms and definitions 3.1.1 ACS reagent grade grade of chemical that meets purity standards as specified by the American Chemical Society (ACS) 3.1.2 user manufacturer, servic
46、e company, end user or operator applying the testing of this part of ISO 13503 3.2 Symbols and abbreviated terms ACS American Chemical Society API American Petroleum Institute ASTM American Society for Testing and Materials CAS Chemical Abstracts Service FCTA first crystal to appear LCTD last crysta
47、l to dissolve NIST National Institute of Standards and Technology NTU nephelometric turbidity unit psi pounds per square inch TCT true crystallization temperature TD to deliver USC United States Customary V volts density, in g/cm3 1 density at lower temperature 2 density at upper temperature 70 dens
48、ity at 70 F (21 C), in lb/gal 21 density at 21 C (70 F), in g/cm3 A-SI average wellbore density, in g/cm3 A-USC average wellbore density, in lb/gal m measured density EN ISO 13503-3:2005 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:20:50 GMT+00:00 2007, Un
49、controlled Copy, (c) BSI 3 cf density, in lb/ft3 SI density, in kg/m3 SI-21 density at 21C, in kg/m3 USC density, in lb/gal W density of water temperature, in C (F) 1 temperature at lower reading, in C (F) 2 temperature at upper reading, in C (F) m measured temperature, in C (F) cf mud gradient, in psi/foot calculated from density expressed in pounds per cubic foot SI mud gradient, in kPa/m USC mud gradient, in psi/foot calculated fro