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1、BRITISH STANDARD BS EN ISO 13500:2006 Petroleum and natural gas industries Drilling fluid ? materials Specifications and tests The European Standard EN ISO 13500:2006 has the status of a British Standard ICS 75.180.10 ? Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006,
2、Uncontrolled Copy, (c) BSI BS EN ISO 13500:2006 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 10 March 2006 BSI 10 March 2006 ISBN 0 580 47944 7 National foreword This British Standard is the official English language version of? EN ISO 135
3、00:2006. It is identical with ISO 13500:2006. It supersedes ? BS EN ISO 13500:1999 which is withdrawn. The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, to Subcommittee PSE/17/-/3, Dri
4、lling and completion fluids and well cements, which has the responsibility to: aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep ? UK interests informed; monitor related internation
5、al and European developments and promulgate them in the UK. A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in
6、 the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsib
7、le for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii to vii, a blank p
8、age, pages 1 to 74, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncont
9、rolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13500 February 2006 ICS 75.180.10Supersedes EN ISO 13500:1998 English Version Petroleum and natural gas industries - Drilling fluid materials - Specifications and tests (ISO 13500:2006) Industries du ptrole et du gaz natur
10、el - Produits pour fluides de forage - Spcifications et essais (ISO 13500:2006) Erdl- und Erdgasindustrie - Bohrsplungen - Spezifikationen und Prfungen (ISO 13500:2006) This European Standard was approved by CEN on 23 January 2006. CEN members are bound to comply with the CEN/CENELEC Internal Regula
11、tions which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This Eur
12、opean Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the nat
13、ional standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Ki
14、ngdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2006 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13500:2006:
15、E Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Foreword This document (EN ISO 13500:2006) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industries“ in collab
16、oration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical
17、 text or by endorsement, at the latest by August 2006, and conflicting national standards shall be withdrawn at the latest by August 2006. This document supersedes EN ISO 13500:1998. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries ar
18、e bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switze
19、rland and United Kingdom. Endorsement notice The text of ISO 13500:2006 has been approved by CEN as EN ISO 13500:2006 without any modifications. EN ISO 13500:2006 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Reference number ISO 13500:200
20、6(E) INTERNATIONAL STANDARD ISO 13500 Second edition 2006-02-15 Petroleum and natural gas industries Drilling fluid materials Specifications and tests Industries du ptrole et du gaz naturel Produits pour fluides de forage Spcifications et essais EN ISO 13500:2006 Licensed Copy: sheffieldun sheffield
21、un, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ii Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 13500:2006 iii Contents Page Foreword vi Introduction vii 1Scope . 1 2Normative references . 1 3Terms, definitio
22、ns, symbols and abbreviations 1 3.1Terms and definitions. 1 3.2Symbols and abbreviations . 2 4Requirements 4 4.1Quality control instructions. 4 4.2Use of test calibration materials in checking testing procedures. 4 4.3Records retention . 4 5Calibration . 4 5.1Coverage 4 5.2Equipment requiring calibr
23、ation . 5 5.3Calibration intervals . 9 6Packaged material 11 6.1Description 11 6.2Apparatus Pallets . 11 6.3Apparatus Bags 11 6.4Marking Pallets . 11 6.5Marking Bags 12 6.6Pallet covers 12 6.7Package weight . 12 6.8Storage. 12 6.9Recycling . 12 7Barite 13 7.1Principle. 13 7.2Reagents and apparatus D
24、ensity by Le Chatelier flask . 13 7.3Procedure Density by Le Chatelier flask . 14 7.4Calculation Density by Le Chatelier flask 15 7.5Reagents and apparatus Water-soluble alkaline earths as calcium. 15 7.6Procedure Water-soluble alkaline earth metals as calcium 16 7.7Calculation Water-soluble alkalin
25、e earths as calcium . 16 7.8Reagents and materials Residue of diameter greater than 75 ?m 16 7.9Procedure Residue of diameter greater than 75 ?m. 17 7.10Calculation Residue of diameter greater than 75 ?m . 17 7.11Reagents and apparatus Particles less than 6 ?m in equivalent spherical diameter by sed
26、imentation method 18 7.12Procedure Particles less than 6 ?m in equivalent spherical diameter by sedimentation method . 18 7.13Calculation Particles less than 6 ?m in equivalent spherical diameter by sedimentation method . 19 8Haematite (hematite) 22 8.1Principle. 22 8.2Reagent and apparatus Density
27、by Le Chatelier flask . 23 8.3Procedure Density by Le Chatelier flask . 23 8.4Calculation Density by Le Chatelier flask 24 8.5Reagents and apparatus Water-soluble alkaline earth metals as calcium 24 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c
28、) BSI EN ISO 13500:2006 iv 8.6Procedure Water-soluble alkaline earth metals as calcium. 25 8.7Calculation Water-soluble alkaline earth metals as calcium . 25 8.8Reagents and apparatus Residues greater that 75 ?m and 45 ?m 26 8.9Procedure Residues of diameter greater than 75 ?m and 45 ?m 26 8.10Calcu
29、lation Residues of diameter greater than 75 ?m and 45 ?m. 27 8.11Reagents and apparatus Particles less than 6 ?m in equivalent spherical diameter by sedimentation method. 27 8.12Procedure Particles less than 6 ?m in equivalent spherical diameter by sedimentation method . 28 8.13Calculation Particles
30、 less than 6 ?m in equivalent spherical diameter by sedimentation method . 28 9Bentonite 31 9.1Principle . 31 9.2Reagents and apparatus Suspension properties . 31 9.3Procedure Rheology of suspension . 31 9.4Calculation Rheology of suspension . 32 9.5Procedure Filtrate volume of suspension 32 9.6Calc
31、ulation Filtrate volume of suspension 33 9.7Reagents and apparatus Residue of diameter greater than 75 ?m. 33 9.8Procedure Residue of diameter greater than 75 ?m . 33 9.9Calculation Residue of diameter greater than 75 ?m . 34 10Non-treated bentonite. 34 10.1Principle . 34 10.2Reagents and apparatus
32、Suspension properties . 34 10.3Procedure Rheology of suspension . 35 10.4Calculation Rheology of suspension . 35 10.5Procedure Dispersed plastic viscosity of suspension. 36 10.6Procedure Dispersed filtrate volume of suspension 36 10.7Calculation Dispersed filtrate volume of suspension 36 11OCMA grad
33、e bentonite . 36 11.1Principle . 36 11.2Reagents and apparatus Suspension properties . 37 11.3Procedure Rheology of suspension . 37 11.4Calculation Rheology of suspension . 38 11.5Procedure Filtrate volume of suspension 38 11.6Calculation Filtrate volume of suspension 38 11.7Reagents and apparatus R
34、esidue of diameter greater than 75 ?m. 39 11.8Procedure Residue of diameter greater than 75 ?m . 39 11.9Calculation Residue of diameter greater than 75 ?m . 39 12Attapulgite 40 12.1Principle . 40 12.2Reagents and apparatus Suspension properties . 40 12.3Procedure 600 r/min dial reading of suspension
35、 41 12.4Reagent and apparatus Residue of diameter greater than 75 ?m. 41 12.5Procedure Residue of diameter greater than 75 ?m . 41 12.6Calculation Residue of diameter greater than 75 ?m . 42 12.7Reagent and apparatus Moisture 42 12.8Procedure Moisture 42 12.9Calculation Moisture 42 13Sepiolite . 43
36、13.1Principle . 43 13.2Reagents and apparatus Suspension properties . 43 13.3Procedure 600 r/min dial reading of suspension 44 13.4Reagents and apparatus Residue of diameter greater than 75 ?m. 44 13.5Procedure Residue of diameter greater than 75 ?m . 44 13.6Calculation Residue of diameter greater t
37、han 75 ?m . 45 13.7Reagents and apparatus Moisture 45 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI v 13.8Procedure Moisture 45 13.9Calculation Moisture 45 14Technical grade low-viscosity CMC (CMC-LVT) 46 14.1Principle. 46 14.2Reagents and
38、 apparatus Determination of starch and starch derivatives. 46 14.3Procedure Determination of starch and starch derivatives. 47 14.4Interpretation Determination of starch and starch derivatives . 47 14.5Reagents and apparatus Solution properties of water-soluble polymers . 48 14.6Procedure Viscometer
39、 reading in deionized water. 48 14.7Procedure Filtrate volume of solution . 49 14.8Calculation Filtrate volume of solution 50 15Technical grade high-viscosity CMC (CMC-HVT) 50 15.1Principle. 50 15.2Reagents and apparatus Determination of starch and starch derivatives. 50 15.3Procedure Determination
40、of starch and starch derivatives. 51 15.4Interpretation Determination of starch and starch derivatives . 52 15.5Reagents and apparatus Solution properties of water-soluble polymers . 52 15.6Procedure Viscometer reading in deionized water. 53 15.7Procedure Viscometer reading in 40 g/l salt water. 53
41、15.8Procedure Viscometer reading in saturated salt water 54 15.9Procedure Filtrate volume of solution . 54 15.10Calculation Filtrate volume of solution 55 16Starch. 55 16.1Principle. 55 16.2Reagents and apparatus Suspension properties. 56 16.3Procedure Viscometer reading in 40 g/l salt water. 56 16.
42、4Procedure Filtrate volume of 40 g/l salt solution 57 16.5Calculation Filtrate volume of 40 g/l salt solution 57 16.6Procedure Viscometer reading in saturated salt solution. 57 16.7Procedure Filtrate volume of saturated salt solution. 58 16.8Calculation Filtrate volume of saturated salt solution. 58
43、 16.9Reagents and apparatus Residue greater than 2 000 ?m 59 16.10Procedure Residue greater than 2 000 ?m 59 Annex A (informative) Mineral impurities in barite . 60 Annex B (informative) Test precision. 61 Annex C (informative) Examples of calculations 66 Bibliography. 74 EN ISO 13500:2006 Licensed
44、Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI vi Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally
45、 carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the w
46、ork. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare Int
47、ernational Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of
48、the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13500 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas indus
49、tries, Subcommittee SC 3, Drilling and completion fluids, and well cements. This second edition cancels and replaces the first edition (ISO 13500:1998), which has been technically revised. EN ISO 13500:2006 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 15:56:16 GMT+00:00 2006, Uncontrolled Copy, (c) BSI v