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1、BRITISH STANDARD BS EN ISO 10426-2:2003 Incorporating amendment no. 1 and corrigendum no. 1 Petroleum and natural gas industries Cements and materials for well cementing Part 2: Testing of well cements The European Standard EN ISO 10426-2:2003, incorporating amendment A1:2005, has the status of a Br
2、itish Standard ICS 75.020; 91.100.10 ? Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI BS EN ISO 10426-2:2003 This British Standard was published under the authority of the Standards Policy and Strategy Committ
3、ee on 16 January 2004 BSI 2007 ISBN 978 0 580 60341 9 National foreword This British Standard is the UK implementation of EN ISO 10426-2:2003, incorporating amendment A1:2005 and corrigendum July 2007. It is identical with ISO 10426-2:2003, incorporating amendment 1:2005 and corrigendum June 2006. T
4、he start and finish of text introduced or altered by corrigendum is indicated in the text by tags . Text altered by ISO corrigendum June 2006 is indicated in the text by . The start and finish of text introduced or altered by ISO amendment is indicated in the text by tags !“. Tags indicating changes
5、 to ISO text carry the number of the ISO amendment. For example, text altered by ISO amendment 1 is indicated by !“. The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, to Subcommittee P
6、SE/17/-/3, Drilling and completion fluids and well cements. A list of organizations represented on this subcommittee can be obtained on request to its secretary. For additional explanatory information please see the National Annex NA at the end of this standard. This publication does not purport to
7、include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publication Amd. No. DateComments 15965March 2006See national foreword 17384 Corrigendum No
8、. 1 31 October 2007See national foreword Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM ICS 75.020; 91.100.10 English version Petroleum and natural gas industr
9、ies - Cements and materials for well cementing - Part 2: Testing of well cements Industries du ptrole et du gaz naturel - Ciments et matriaux pour la cimentation des puits - Partie 2: Essais CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for
10、giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official ver
11、sions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATIO
12、N EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2003 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. EN ISO 10426-2 October 2003 +A1 September 2005 (ISO 10426-2:2003) de ciments pour puits (ISO 10426-2:20
13、03) Erdl- und Erdgasindustrie - Zemente und Materialien fr die Zementation von Tiefbohrungen - Teil 2: Prfungen fr Bohrloch-Zemente (ISO 10426-2:2003) Ref. No. EN ISO 10426-2:2003 E This European Standard was approved by CEN on 1 October 2003. CEN members are the national standards bodies of Austria
14、, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Incorporating corrigendum July 2007
15、 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI Foreword This document (EN ISO 10426-2:2003) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and n
16、atural gas industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publicatio
17、n of an identical text or by endorsement, at the latest by April 2004, and conflicting national standards shall be withdrawn at the latest by April 2004. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Eur
18、opean Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and the United Kingdom. NOTE FROM CMC The foreword is susceptible to be amended on rec
19、eption of the German language version. The confirmed or amended foreword, and when appropriate, the normative annex ZA for the references to international publications with their relevant European publications will be circulated with the German version. Endorsement notice The text of ISO 10426-2:200
20、3 has been approved by CEN as EN ISO 10426-2:2003 without any modifications. EN ISO 104262:2003 Foreword to amendment A1 This document (EN ISO 10426-2:2003/A1:2005) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas industri
21、es“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical t
22、ext or by endorsement, at the latest by March 2006, and conflicting national standards shall be withdrawn at the latest by March 2006. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Aus
23、tria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Endorsement notice The text of
24、ISO 10426-2:2003 has been approved by CEN as EN ISO 10426-2:2003/A1:2005 without any modifications. Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI Reference number ISO 10426-2:2003(E) NINRETOITALAN ADNATSDR IS
25、O 162402- tide tsriFino -300251-01 Petroleum and natural gas industries Cements and materials for well cementing Part 2: Testing of well cements Industries du ptrole et du gaz naturel Ciments et matriaux pour la cimentation des puits Partie 2: Essais de ciment pour puits INTERNATIONAL STANDARD ISO 1
26、0426-2 First edition 2003-10-15 EN ISO 104262:2003 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI ii Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 200
27、7, Uncontrolled Copy, (c) BSI iii Contents Page Forewordvi Introduction vii 1Scope1 2Normative references .1 3Terms, definitions and symbols1 3.1Terms and definitions.1 3.2Symbols .7 4Sampling8 4.1General.8 4.2Sampling cement at field location.8 4.3Sampling cement blends at field location8 4.4Sampli
28、ng dry cement additives at field location .8 4.5Sampling liquid cement additives at field location .8 4.6Sampling mixing water.8 4.7Shipping and storage .10 4.8Sample preparation prior to testing10 4.9Sample disposal10 5Preparation of slurry.10 5.1General.10 5.2Apparatus.10 5.3Procedure.12 6Determin
29、ation of slurry density.14 6.1Preferred apparatus14 6.2Calibration14 6.3Procedure.14 6.4Alternative apparatus and procedure .16 7Well-simulation compressive strength tests16 7.1General.16 7.2Sampling16 7.3Preparation of slurry.17 7.4Apparatus.17 7.5Procedure.18 7.6Determination of cement compressive
30、 strength at the top of long cement columns .20 8Non-destructive sonic testing of cement .26 8.1General.26 8.2Apparatus.26 8.3Sampling26 8.4Preparation of slurry.26 8.5Procedure.26 8.6Curing time 26 8.7Curing schedules26 8.8Data reporting27 9Well-simulation thickening-time tests 27 9.1General.27 9.2
31、Apparatus and material27 9.3Calibration28 9.4Test procedure 30 EN ISO 104262:2003 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI iv 9.5Determination of test schedule32 10Static fluid-loss tests 38 10.1General
32、.38 10.2Apparatus.38 10.3Safety39 10.4Mixing procedure.39 10.5Conditioning procedures39 10.6Procedures for testing at temperatures u u u u 88 ? ? ? ?C (190 ? ? ? ?F)39 10.7Procedures for testing at temperatures ? ? ? ? 88 ? ? ? ?C (190 ? ? ? ?F).40 10.8Filling the static fluid-loss cell.42 10.9Fluid
33、 loss test 43 10.10Test completion and clean-up43 11Permeability tests45 11.1General .45 11.2Apparatus.45 11.3Sample preparation.46 11.4Liquid permeability (cement permeameter)46 11.5Alternative procedure (core permeameter) for liquid permeability47 11.6Calculating liquid permeability50 11.7Gas perm
34、eability (core permeameter).50 11.8Calculating gas permeability51 12Determination of rheological properties and gel strength using a rotational viscometer 52 12.1General .52 12.2Apparatus.52 12.3Calibration54 12.4Determination of rheological properties.54 12.5Determination of gel strength56 12.6Mode
35、lling of the rheological behaviour 57 13Calculation of pressure drop and flow regime for cement slurries in pipes and annuli .65 13.1General .65 13.2Newtonian fluids67 13.3Power Law fluids.71 13.4Bingham Plastic fluids77 13.5Conversion factors87 14Test procedure for arctic cementing slurries.87 14.1
36、General .87 14.2Preparation of cement slurry .87 14.3Fluid fraction87 14.4Thickening time.87 14.5Compressive strength 87 14.6Freeze-thaw cycling at atmospheric pressure .88 14.7Compressive strength cyclic testing.88 15Well-simulation slurry stability tests.88 15.1Introduction88 15.2Slurry mixing89 1
37、5.3Slurry conditioning89 15.4Free-fluid test with heated static period .89 15.5Free-fluid test with ambient temperature static period.90 15.6Sedimentation test 90 16Compatibility of wellbore fluids.94 16.1General .94 16.2Preparation of test fluids94 16.3Rheology95 16.4Thickening time.95 16.5Compress
38、ive strength 95 16.6Solids suspension and static gel strength.95 EN ISO 104262:2003 Licensed Copy: London South Bank University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI v 16.7Fluid loss95 17Pozzolans.98 17.1General.98 17.2Types of pozzolan.98 17.3
39、Physical and chemical properties.98 17.4Slurry calculations99 17.5Bulk volume of a blend.100 Annex A (normative) Procedure for preparation of large slurry volumes102 Annex B (normative) Calibration procedures for thermocouples, temperature-measuring systems and controllers 104 Annex C (informative)
40、Additional information relating to temperature determination106 Annex D (normative) Alternative apparatus for well thickening-time tests .113 Annex E (informative) Cementing schedules 116 Bibliography .171 EN ISO 104262:2003 16.8Water-wetting capability test (WWCT) 95 Licensed Copy: London South Ban
41、k University, London South Bank University, Wed Oct 17 01:21:06 GMT+00:00 2007, Uncontrolled Copy, (c) BSI vi Foreword ISO (the International Organisation for Standardisation) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is
42、 normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organisations, governmental and non-governmental, in liaison with ISO, also take part
43、 in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardisation. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. Draft International Standards adopted by the t
44、echnical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. I
45、SO shall not be held responsible for identifying any or all such patent rights. ISO 10426-2 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids and well
46、cements. ISO 10426 consists of the following parts, under the general title Petroleum and natural gas industries Cements and materials for well cementing: ? Part 1: Specification ? Part 2: Testing of well cements ? Part 3: Testing of deepwater well cement formulations ? Part 4: Preparation and testi
47、ng of foamed cement slurries at atmospheric pressure The following part is under preparation: ? Part 5: Determination of shrinkage and expansion of well cement formulations at atmospheric pressure EN ISO 104262:2003 Foreword to amendment A1 ISO (the International Organization for Standardization) is
48、 a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represen
49、ted on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standa