《BS-EN-ISO-13503-2-2006.pdf》由会员分享，可在线阅读，更多相关《BS-EN-ISO-13503-2-2006.pdf（40页珍藏版）》请在三一文库上搜索。
1、BRITISH STANDARD BS EN ISO 13503-2:2006 Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations The European Standard EN ISO 13503-2:2006 has the status of a British Standard ICS 75
2、.100 ? Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 13503-2:2006 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 November 2006 BSI 2006
3、ISBN 0 580 49689 9 National foreword This British Standard was published by BSI. It is the UK implementation of EN ISO 13503-2:2006. The UK participation in its preparation was entrusted by Technical Committee PSE/17, Materials and equipment for petroleum, petrochemical and natural gas industries, t
4、o Subcommittee PSE/17/-/3, Drilling and completion fluids and well cements. A list of organizations represented on PSE/17/-/3 can be obtained on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct ap
5、plication. Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publication Amd. No. DateComments Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN ST
6、ANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13503-2 November 2006 ICS 75.100 English Version Petroleum and natural gas industries - Completion fluids and materials - Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations (ISO 13503-2:2006) Industr
7、ies du ptrole et du gaz naturel - Fluides de compltion et matriaux - Partie 2: Mesurage des proprits des matriaux de soutnement utiliss dans les oprations de fracturation hydraulique et de remplissage de gravier (ISO 13503-2:2006) Erdl- und Erdgasindustrie - Komplettierungsflssigkeiten und -material
8、ien - Teil 2: Messung der Eigenschaften von Sttzmaterialien zum Einsatz bei hydraulischen Fraktionierungs- und in Kiespackungsvorgngen (ISO 13503-2:2006) This European Standard was approved by CEN on 22 September 2006. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which s
9、tipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standar
10、d exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standar
11、ds bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPE
12、AN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2006 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13503-2:2006: E Licensed
13、Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Foreword This document (EN ISO 13503-2:2006) has been prepared by Technical Committee ISO/TC 67 “Materials, equipment and offshore structures for petroleum and natural gas
14、 industries“ in collaboration with Technical Committee CEN/TC 12 “Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries“, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publi
15、cation of an identical text or by endorsement, at the latest by May 2007, and conflicting national standards shall be withdrawn at the latest by May 2007. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this Eu
16、ropean Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. En
17、dorsement notice The text of ISO 13503-2:2006 has been approved by CEN as EN ISO 13503-2:2006 without any modifications. EN ISO 13503-2:2006 Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Reference number ISO
18、13503-2:2006(E) INTERNATIONAL STANDARD ISO 13503-2 First edition 2006-11-01 Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations Industries du ptrole et du gaz naturel Fluides de
19、 compltion et matriaux Partie 2: Mesurage des proprits des matriaux de soutnement utiliss dans les oprations de fracturation hydraulique et de remplissage de gravier EN ISO 13503-2:2006 Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Unc
20、ontrolled Copy, (c) BSI ii Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI iii Contents Page Foreword. v Introduction. vi 1 Scope . 1 2 Normative references. 1 3 Abbreviations 1 4 Standard proppant sampling pro
21、cedure 2 4.1 General. 2 4.2 Particle segregation 2 4.3 Equipment . 2 4.4 Number of required samples Bulk 4 4.5 Sampling Bulk material 5 4.6 Sampling Bagged material 5 5 Sample handling and storage 5 5.1 Sample reduction 5 5.2 Sample splitting 5 5.3 Sample and record retention and storage . 5 6 Sieve
22、 analysis . 6 6.1 Purpose 6 6.2 Description 6 6.3 Equipment and materials. 6 6.4 Procedure 6 6.5 Calculation of the mean diameter, median diameter and standard deviation 7 6.6 Sieve calibration . 9 7 Proppant sphericity and roundness. 11 7.1 Purpose 11 7.2 Description 12 7.3 Apparatus capability. 12
23、 7.4 Procedure 12 7.5 Alternate method for determining average sphericity and roundness. 13 8 Acid solubility . 13 8.1 Purpose 13 8.2 Description 13 8.3 Equipment and materials. 14 8.4 Procedure 14 9 Turbidity test . 15 9.1 Purpose 15 9.2 Description 16 9.3 Equipment and materials. 16 9.4 Equipment
24、calibration 16 9.5 Procedure 16 10 Procedures for determining proppant bulk density, apparent density and absolute density 17 10.1 Purpose 17 10.2 Description 17 10.3 Bulk density. 17 10.4 Apparent density. 19 10.5 Absolute density. 21 EN ISO 13503-2:2006 Licensed Copy: London South Bank University,
25、 London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI iv 11 Proppant crush-resistance test.21 11.1 Purpose21 11.2 Description.21 11.3 Equipment and materials .22 11.4 Sample preparation.22 11.5 Crush-resistance procedure23 12 Loss on ignition of resin-coated p
26、roppant.25 12.1 Objective25 12.2 Apparatus and materials25 12.3 Loss-on-ignition procedure for whole-grain proppant .25 Annex A (informative) Formazin solution preparation27 Bibliography .28 EN ISO 13503-2:2006 Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:
27、44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI v Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Eac
28、h member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the Internation
29、al Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standard
30、s adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject o
31、f patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13503-2 was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completio
32、n fluids, and well cements. ISO 13503 consists of the following parts, under the general title Petroleum and natural gas industries Completion fluids and materials: Part 1: Measurement of viscous properties of completion fluids Part 2: Measurement of properties of proppants used in hydraulic fractur
33、ing and gravel-packing operations Part 3: Testing of heavy brines Part 4: Procedure for measuring stimulation and gravel-pack fluid leakoff under static conditions Part 5: Procedures for measuring the long-term conductivity of proppants EN ISO 13503-2:2006 Licensed Copy: London South Bank University
34、, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI vi Introduction This part of ISO 13503 is a compilation and modification of API RP 56 1, API RP 58 2 and API RP 60 3. The procedures have been developed to improve the quality of proppants delivered to the
35、 well site. They are for use in evaluating certain physical properties used in hydraulic fracturing and gravel-packing operations. These tests should enable users to compare the physical characteristics of various proppants tested under the described conditions and to select materials useful for hyd
36、raulic fracturing and gravel-packing operations. The procedures presented in this part of ISO 13503 are not intended to inhibit the development of new technology, material improvements or improved operational procedures. Qualified engineering analysis and judgment are required for their application
37、to a specific situation. In this part of ISO 13503, where practical, US Customary (USC) units are included in brackets for information. Annex A of this part of ISO 13503 is for information only. EN ISO 13503-2:2006 Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24
38、 04:44:54 GMT+00:00 2006, Uncontrolled Copy, (c) BSI 1 Petroleum and natural gas industries Completion fluids and materials Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel-packing operations 1 Scope This part of ISO 13503 provides standard testing procedures fo
39、r evaluating proppants used in hydraulic fracturing and gravel-packing operations. NOTE “Proppants” mentioned henceforth in this part of ISO 13503 refer to sand, ceramic media, resin-coated proppants, gravel-packing media and other materials used for hydraulic fracturing and gravel-packing operation
40、s. The objective of this part of ISO 13503 is to provide a consistent methodology for testing performed on hydraulic fracturing and/or gravel-packing proppants. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, onl
41、y the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ASTM E11, Standard Specification for Wire Cloth and Sieves for Testing Purposes 3 Abbreviations API American Petroleum Institute ASTM American Society for Testing an
42、d Materials ASG apparent specific gravity FTU formazin turbidity unit HCI hydrochloric acid HF hydrofluoric acid LOI loss on ignition NTU nephelometric turbidity unit EN ISO 13503-2:2006 Licensed Copy: London South Bank University, London South Bank University, Sun Dec 24 04:44:54 GMT+00:00 2006, Un
43、controlled Copy, (c) BSI 2 4 Standard proppant sampling procedure 4.1 General Before any sample is taken, consider what tests will be performed, as each test requires a different volume. It is very important that both the supplier and customer obtain the best representative sample possible. Unless t
44、he sample is truly representative of a total shipment or container, testing and correlation with specifications/standards is very difficult. It is unlikely that sampling/testing methods in the field duplicate the producers system. The standard procedures included within this part of ISO 13503 are to
45、 assist in obtaining representative samples. However, there are inherent variations associated with sampling, testing equipment and the procedures that can lead to inconsistent results. A sample that is representative of a truckload 23 000 kg (50 700 lb) or a railcar load 90 000 kg (198 000 lb) can
46、be an initial source of wide variation when making comparisons. All parties shall take care to insure uniform sampling. The customer and the supplier shall agree on sampling and testing methods/techniques. For the best representation, continuous sampling is ideal. Although many proppant suppliers ut
47、ilize automatic sampling, it is usually impractical at the job site. If sampling is conducted while unloading a container or at the site, consideration should be given to the number or frequency of samples. If bulk containers are filled from a flowing stream of proppant material, sampling procedures
48、 in accordance with 4.5 shall be applied. If bulk containers are filled using sacked proppant material, sampling procedures in accordance with 4.6 shall be applied. 4.2 Particle segregation It is important to have a basic understanding of segregation when sampling proppant. Depending on the size, sh
49、ape, distribution and mechanisms involved, there is usually a certain amount of error or variability involved in sampling due to segregation. The sampling procedures described here are the result of much experience and are designed to minimize the effects of segregation of particles by size. Particles, such as proppants, naturally find the path of least resistance when moved or when force is applied. During transfer or movement, particles of differ