《ISO-13503-3-2005.pdf》由会员分享，可在线阅读，更多相关《ISO-13503-3-2005.pdf（53页珍藏版）》请在三一文库上搜索。
1、ICS 75.100 Ref. No. ISO 13503-3:2005/Cor.1:2006(E) ISO 2006 All rights reserved Published in Switzerland INTERNATIONAL STANDARD ISO 13503-3:2005/Cor.1:2006(E) TECHNICAL CORRIGENDUM 1 Published 2006-04-01 INTERNATIONAL ORGANIZATION FOR STANDARDIZATION ORGANISATION INTERNATIONALE DE NORMALISATION Petr
2、oleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy brines TECHNICAL CORRIGENDUM 1 Industries du ptrole et du gaz naturel Fluides et matriaux de compltion Partie 3: Essais de saumures denses RECTIFICATIF TECHNIQUE 1 Technical Corrigendum 1 to ISO 13503-3 was pre
3、pared by Technical Committee ISO/TC 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. French title on the cover Replace the second part of the title “Fluides et matriaux de co
4、mpltion” with “Fluides de compltion et matriaux”. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-
5、,- Reference number ISO 13503-3:2005(E) ISO 2005 INTERNATIONAL STANDARD ISO 13503-3 First edition 2005-12-15 Petroleum and natural gas industries Completion fluids and materials Part 3: Testing of heavy brines Industries du ptrole et du gaz naturel Fluides et matriaux de compltion Partie 3: Essais d
6、e saumures denses Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) PDF discl
7、aimer This PDF file may contain embedded typefaces. In accordance with Adobes licensing policy, this file may be printed or viewed but shall not be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this file, parties a
8、ccept therein the responsibility of not infringing Adobes licensing policy. The ISO Central Secretariat accepts no liability in this area. Adobe is a trademark of Adobe Systems Incorporated. Details of the software products used to create this PDF file can be found in the General Info relative to th
9、e file; the PDF-creation parameters were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event that a problem relating to it is found, please inform the Central Secretariat at the address given below. ISO 2005 All ri
10、ghts reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISOs member body in the country of t
11、he requester. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. + 41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org Published in Switzerland ii ISO 2005 All rights reserved Copyright International Organization for Standardization Provided by IHS under license wi
12、th ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) ISO 2005 All rights reserved iii Contents Page Foreword. v Introduction. vi 1 Scope . 1 2 Normative references. 1 3
13、Terms, definitions and abbreviated terms . 2 3.1 Terms and definitions. 2 3.2 Symbols and abbreviated terms . 2 4 Requirements 4 4.1 Quality control instructions. 4 4.2 Records retention. 4 5 Calibration of equipment . 4 5.1 General requirements. 4 5.2 Reagents and materials for calibration 4 5.3 Ge
14、neral requirements for calibration of particular apparatus . 5 5.4 Frequency of calibration verification 5 5.5 Calibration verification. 6 6 Density. 7 6.1 General. 7 6.2 Apparatus 9 6.3 Density measurement by hydrometer 10 6.4 Density correction to 21 C (70 F) 11 6.5 Calculation of density in units
15、 other than kg/m3. 13 6.6 Calculation for pressure and temperature compensation 14 7 Crystallization temperature . 16 7.1 Principle. 16 7.2 Apparatus 20 7.3 Determination of crystallization point 21 7.4 Calculation of crystallization point. 21 8 Brine clarity. 22 8.1 Principle. 22 8.2 Apparatus 22 8
16、.3 Determination of brine clarity 23 9 Solids evaluation by gravimetric procedures 23 9.1 Principle. 23 9.2 Apparatus 24 9.3 Preparation of glass-fibre filter disk. 24 9.4 Selection of sample volume 25 9.5 Determination of total suspended solids. 25 9.6 Calculation of total suspended solids 26 9.7 C
17、alculation of precision and bias . 26 9.8 Determination of volatile and non-volatile solids 26 9.9 Calculation of non-volatile and volatile solids 27 10 pH . 27 10.1 Principle. 27 10.2 Reagents and materials . 28 10.3 Apparatus 28 10.4 Measurement of pH. 29 Copyright International Organization for S
18、tandardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) iv ISO 2005 All rights reserved 10.5 Precision statement30 10.6 Care
19、of the electrode 30 11 Iron contamination30 11.1 Principle.30 11.2 Reagents and materials31 11.3 Apparatus.31 11.4 Preparation of colorimetric standards32 11.5 Measurement of iron contamination.32 11.6 Precision statement33 12 Daily completion fluid report .33 12.1 Principle.33 12.2 Well identificat
20、ion, geometry and zone data34 12.3 System properties.34 12.4 Fluids accounting .35 12.5 Cost accounting35 12.6 Daily commentary .35 12.7 Vendor representative identification.35 Annex A (informative) Completion fluids report form.36 Annex B (informative) Gas hydrates.37 Annex C (informative) Bufferin
21、g capacity of brines38 Annex D (informative) Pressure crystallization of brines.39 Annex E (informative) Brine viscosity40 Annex F (informative) Principle of corrosion testing41 Bibliography .43 Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=
22、NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) ISO 2005 All rights reserved v Foreword ISO (the International Organization for Standardization) is a worldwide federation of nation
23、al standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. Internatio
24、nal organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rule
25、s given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at l
26、east 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13503-3 was prepared by Technical Committee ISO/TC
27、 67, Materials, equipment and offshore structures for petroleum, petrochemical and natural gas industries, Subcommittee SC 3, Drilling and completion fluids, and well cements. ISO 13503 consists of the following parts, under the general title Petroleum and natural gas industries Completion fluids an
28、d materials: Part 1: Measurement of viscous properties of completion fluids Part 3: Testing of heavy brines The following parts are under preparation: Part 2: Measurement of properties of proppants used in hydraulic fracturing and gravel packing operations Part 4: Procedure for measuring stimulation
29、 and gravel-pack fluid leakoff under static conditions Part 5: Procedure for measuring the long-term conductivity of proppants Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:
30、16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) vi ISO 2005 All rights reserved Introduction This part of ISO 13503 covers heavy brines commonly used in petroleum and natural gas completion, workover and drill-in fluids. These brines can be purchas
31、ed or rented from multiple sources, and are available worldwide. No single source or limited source of supply is included, either by inference or reference. Annexes A to F are given for information. Copyright International Organization for Standardization Provided by IHS under license with ISO Licen
32、see=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- INTERNATIONAL STANDARD ISO 13503-3:2005(E) ISO 2005 All rights reserved 1 Petroleum and natural gas industries Completion fluids and materials Part
33、3: Testing of heavy brines 1 Scope This part of ISO 13503 covers the physical properties, potential contaminants and test procedures for heavy brine fluids manufactured for use in oil and gas well drilling, completion and workover fluids. This part of ISO 13503 provides methods for assessing the per
34、formance and physical characteristics of heavy brines for use in field operations. It includes procedures for evaluating the density or specific gravity, the clarity or amount of particulate matter carried in the brine, the crystallization point or the temperature (both ambient and under pressure) a
35、t which the brines make the transition between liquid and solid, the pH, and iron contamination. It also contains a discussion of gas hydrate formation and mitigation, brine viscosity, corrosion testing, buffering capacity and a standardised reporting form. This part of ISO 13503 is intended for the
36、 use of manufacturers, service companies and end-users of heavy brines. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced
37、 document (including any amendments applies). ISO 10414-1:2001, Petroleum and natural gas industries Field testing of drilling fluids Part 1: Water-based fluids ASTM 1) E77, Standard Test Method for Inspection and Verification of Thermometers NIST 2) SRM 185h, Potassium Hydrogen Phthalate, pH Standa
38、rd NIST SRM 186g, Potassium Dihydrogen Phosphate, pH Standard NIST SRM 191C, pH Standards NBS (NIST) Circular 555, Testing of Hydrometers, 22 Oct 1954 1) ASTM, American Society for Testing and Materials, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, USA. http:/www.astm.org.
39、 2) NIST, National Institute of Standards and Technology, 100 Bureau Drive, Stop 3460, Gaithersburg, MD 20899-3460, USA. http:/www.nist.gov. Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale,
40、04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005(E) 2 ISO 2005 All rights reserved 3 Terms, definitions and abbreviated terms For the purposes of this document, the following terms, definitions and abbreviated terms apply. 3.1 Terms and d
41、efinitions 3.1.1 ACS reagent grade grade of chemical that meets purity standards as specified by the American Chemical Society (ACS) 3.1.2 user manufacturer, service company, end user or operator applying the testing of this part of ISO 13503 3.2 Symbols and abbreviated terms ACS American Chemical S
42、ociety API American Petroleum Institute ASTM American Society for Testing and Materials CAS Chemical Abstracts Service FCTA first crystal to appear LCTD last crystal to dissolve NIST National Institute of Standards and Technology NTU nephelometric turbidity unit psi pounds per square inch TCT true c
43、rystallization temperature TD to deliver USC United States Customary V volts density, in g/cm3 1 density at lower temperature 2 density at upper temperature 70 density at 70 F (21 C), in lb/gal 21 density at 21 C (70 F), in g/cm3 A-SI average wellbore density, in g/cm3 A-USC average wellbore density
44、, in lb/gal m measured density Copyright International Organization for Standardization Provided by IHS under license with ISO Licensee=NASA Technical Standards 1/9972545001 Not for Resale, 04/07/2007 02:16:42 MDTNo reproduction or networking permitted without license from IHS -,-,- ISO 13503-3:2005
45、(E) ISO 2005 All rights reserved 3 cf density, in lb/ft3 SI density, in kg/m3 SI-21 density at 21C, in kg/m3 USC density, in lb/gal W density of water temperature, in C (F) 1 temperature at lower reading, in C (F) 2 temperature at upper reading, in C (F) m measured temperature, in C (F) cf mud gradi
46、ent, in psi/foot calculated from density expressed in pounds per cubic foot SI mud gradient, in kPa/m USC mud gradient, in psi/foot calculated from density expressed in pounds per gallon Bc intercept of hydrometer-correction curve C density correction factor for temperature, in g/cm3 per C C tempera
47、ture correction factor, in lb/gal per 100 F Cp pressure correction factor, in lb/gal per 1 000 psi CSI density correction factor for temperature, in kg/m3 per C CUSC density correction factor for temperature, in lb/gal per F h depth (height) of well, in feet h2 depth (height) of well at true vertica
48、l depth, in feet R hydrometer reading, specific gravity R1 hydrometer reading at lower temperature R2 hydrometer reading at higher temperature V volume, in cm3 V1 volume of the original sample, in cm3 Zc slope of hydrometer-correction curve Copyright International Organization for Standardization Provided by IHS unde