1、ISOInternationalStandardISO19674Secondedition2025-06Fineceramics(advancedceramics,advancedtechnicalceramics)一MethodsoftestforceramiccoatingsDeterminationofinternalstressinceramiccoatingsbyapplicationoftheStoneyformulaCeramiquesfines(ceramiquesavancees,Ceramiquestechniquesavancees)Methodesdessaidesre
2、velementsceramiquesDeterminationdelaContrainteinternedesrevetementsceramiquesparapplicationdelaformuledeStoneyReferencenumberISO19674:2025(en)COPYRIGHTPROTECTEDDOCUMENTISO2025Allrightsreserved.Unlessotherwisespecified,orrequiredinthecontextofitsimplementation,nopartofthispublicationmaybereproducedor
3、utilizedotherwiseinanyformorbyanymeans,electronicormechanical,includingphotocopying,orpostingontheinternetoranintranet,withoutpriorwrittenpermission.PermissioncanberequestedfromeitherISOattheaddressbeloworISO,smemberbodyinthecountryoftherequester.ISOcopyrightofficeCP401Ch.deBlandonnet8CH-1214Vernier
4、GenevaPhone:+41227490111Email:copyrightiso.orgWebsite:www.iso.orgPublishedinSwitzerlandPageContentsForewordivIntroductionv1 Scope12 Normativereferences13 Termsanddefinitions14 Principle15 Apparatus26 Preparationoftestspecimens36.1 Material36.2 Samplegeometry36.3 Samplesurfacefinish36.4 Sampledimens
5、ions31234567ZZ7.ZZZZMeasuringrangeandinitialprofile4Depositionofthecoating4Coatingthickness5Adjustingthesamplegeometryafterdepositionofthecoating5Measuringthefinalprofile5Calculationofstress67.6.1 fhs0,0267.6.2 0f02hfh0,17Numberofrepeatmeasurements78 Limitstomethod79 Testreport7Annex A (informative)
6、Determinationofsuitabledimensionsforthetestsample9Annex B (informative)Internalstresscalculationinceramiccoatingofrealcomponents11Bibliography13ForewordISO(theInternationalOrganizationforStandardization)isaworldwidefederationofnationalstandardsbodies(ISOmemberbodies).TheworkofpreparingInternationalS
7、tandardsisnormallycarriedoutthroughISOtechnicalcommittees.Eachmemberbodyinterestedinasubjectforwhichatechnicalcommitteehasbeenestablishedhastherighttoberepresentedonthatcommittee.Internationalorganizations,governmentalandnon-governmental,inliaisonwithISO,alsotakepartinthework.ISOcollaboratescloselyw
8、iththeInternationalElectrotechnicalCommission(IEC)onallmattersofelectrotechnicalstandardization.TheproceduresusedtodevelopthisdocumentandthoseintendedforitsfurthermaintenancearedescribedintheISO/IECDirectives,Part1.Inparticular,thedifferentapprovalcriterianeededforthedifferenttypesofISOdocumentsshou
9、ldbenoted.ThisdocumentwasdraftedinaccordancewiththeeditorialrulesoftheISO/IECDirectives,Part2(seeWWW.iso.org/directives).ISOdrawsattentiontothepossibilitythattheimplementationofthisdocumentmayinvolvetheuseof（八）patent(三).ISOtakesnopositionconcerningtheevidence,validityorapplicabilityofanyclaimedpaten
10、trightsinrespectthereof.Asofthedateofpublicationofthisdocument,ISOhadnotreceivednoticeof（八）patent(三)whichmayberequiredtoimplementthisdocument.However,Implementersarecautionedthatthismaynotrepresentthelatestinformation,whichmaybeobtainedfromthepatentdatabaseavailableatWWW.iso.org/patents.ISOshallnotb
11、eheldresponsibleforidentifyinganyorallsuchpatentrights.Anytradenameusedinthisdocumentisinformationgivenfortheconvenienceofusersanddoesnotconstituteanendorsement.Foranexplanationofthevoluntarynatureofstandards,themeaningofISOspecifictermsandexpressionsrelatedtoconformityassessment,aswellasinformation
12、aboutISOsadherencetotheWorldTradeOrganization(WTO)principlesintheTechnicalBarrierstoTrade(TBT),seeWWW.iso.org/iso/foreword.htmLThisdocumentwaspreparedbyTechnicalCommitteeISO/TC206,Fineceramics.Thissecondeditioncancelsandreplacesthefirstedition(ISO19674:2017),whichhasbeentechnicallyrevised.Themaincha
13、ngesareasfollows: intheScope,thesubstrateislimitedtoisotropicones; inClause5,thecontentsofEXAMPLEarealldeletedduetoanincorrectFOlmUlaanditsweakcorrelation;一in7.5,thecalculationforRaYnhasbeenrevised; attheendofZ15aschematicdiagram(Figure1)andanapproximatecalculationofReXPfromdeflectionhasbeenaddedand
14、theformularenumberedtoFormula(3); AnneXBhasbeenadded.Anyfeedbackorquestionsonthisdocumentshouldbedirectedtotheusersnationalstandardsbody.AcompletelistingofthesebodiescanbefoundatWWW.iso.org/members.htmLIntroductionThereisanincreasinguseofcoatingstoimprovethefunctionalperformanceofmaterialsandcompone
15、nts.Thiscanbetoprotectagainstdamageduetoexposuretodemandingenvironmentsincludinghighstressesandaggressivechemicalenvironments,butcanalsobetomodifymanyotherproperties,e.g.thermalconductivitythroughthermalbarriercoatings,frictionthroughlowfrictioncoatings,suchasdiamondlikecarbon(DLC工andopticalreflecti
16、vitythroughcoatingswithcontrolledopticalproperties.Appropriatechoiceofcoatingsforparticularapplicationsdependsonthemechanicalandotherfunctionalrequirementsthatarise.Onefactorthatcanbecrucialindeterminingcoatingperformanceandlifetimeistheresidualstressthatisgeneratedbythedepositionprocessand/orbyther
17、malexpansionmismatchbetweenthecoatingandthesubstrateasthecomponentiscooledfromtheprocessingtemperature.ThisdocumentdescribestheapplicationofasimpleexperimentaltechniqueusingtheStoneyformulatoanalysethecoatinginducedbendingofcoupons,ofknownmechanicalproperties,todeterminetheresidualstressinthecoating
18、Fineceramics(advancedceramics,advancedtechnicalceramics)Methodsoftestforceramiccoatings一DeterminationofinternalstressinceramiccoatingsbyapplicationoftheStoneyformula1 ScopeThisdocumentspecifiesamethodfordeterminationoftheinternalstressinthinceramiccoatings.Theinternalstressisdeterminedbyapplication
19、oftheStoneyformulatotheresultsobtainedfrommeasurementoftheradiusofcurvatureofisotropicstripsordiscswithsingle-facecoating.2 NormativereferencesTherearenonormativereferencesinthisdocument.3 TermsanddefinitionsNotermsanddefinitionsarelistedinthisdocumentISOandIECmaintainterminologydatabasesforuseinsta
20、ndardizationatthefollowingaddresses: ISOOnlinebrowsingplatform:availableathttps:WWW.iso.org/obp IECElectropedia:availableathttps:WWW.electropedia.org/4PrincipleCoatingstressoftenplaysamajorroleintheperformanceofcoatedtoolsandmachineparts.Differenttechniqueshavebeendevelopedforthedeterminationofcoati
21、ngstress.Thetechniqueconsideredinthisdocumentcalculatesthestressfrommeasurementofthebowingofthindiscsorstripsofwell-characterizedmaterialsofknownthicknessthathavebeencoatedononesideonly.Itisassumedthatthedeformationiselastic,i.e.ifthecoatingweretoberemovedthesubstratewouldreturntoitsinitialshape.Pro
22、videdthatthecoatingisthincomparedtothethicknessofthesubstrate(coatingthickness20m)radiiofcurvatureusingopticaltechniques.Beforemeasuringtheinitialprofile,defineameasuringrange(lengthA),alongthelengthaofthesubstrate(alongadiameterforthedisc).Inordertoavoidanyedgeeffects,themeasuringrangeshouldstopata
23、distancefromtheendsequaltoatleast20timesthesamplethickness.Makesomereferencemarks,e.g.Vickersindentations,onthesubstratealongastraightlineatlengthdirection,sothatthefinalprofilecanbemeasuredatthesamelocationandinthesamedirectionastheinitialone.Thisprocedureisessentialwhentheinitialprofileissomewhatd
24、ifferentfromaperfectcircle.Itisrecommendedthat,wherehardnessindentsareusedasreferencemarks,indentationsshouldbeproducedusingamicrohardnesstesterataloadofnogreaterthan1kg.Formeasuringtheprofile,thesampleshallliefreely,withoutanyexternalstress.Placethestripontwosupports,sothatitoverhangseachsupportbya
25、quarterofitslength;proceedsimilarlyforadisc.NOTEInmanycases,supportingthesampleonitsendswillhavenegligibleeffectuponthecurvature.However,theuseofsupportswillavoidproblemswithstabilityofthesampleifoneorbothendsofthesamplearenotperpendiculartothesides.Especiallyforthinsamples,ensurethattheweightofthes
26、ampledoesnotchangeitsshape:turningthestrip(ordisc)overonthesupportsshouldleavetheprofileunchanged,exceptforthesign.Inthecaseofopticalmicroscopy,foreachprofile,measurethecoordinates(Xfzi)ofabout10pointsdistributeduniformlyalongthepredefinedmeasuringrange.Theordinatezicorrespondstotheverticalpositiono
27、fthemicroscopeobjectiveforwhichthepointxiofthesurfaceofthesampleisintheimageplane.Thefocusingaxisofthemicroscopeshallbeperpendiculartothesurfacetobecoated,andespeciallytoitslongitudinalaxis.Theinitialcurvaturecanbedisregardedinsofarasitisverylow(5%)whencomparedwiththefinalcurvature.Aftertheinitialprofileismeasured,thesampleshallbehandledinsuchawayastoavoidchangesininternalstressorinirreversibledeformation.7.2 DepositionofthecoatingThetestmethodreliesupontheco
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