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1、BRITISH STANDARD BS EN 13516:2002 Incorporating Corrigendum No. 1 Footwear Test methods for uppers, lining and insocks Colour fastness to rubbing The European Standard EN 13516:2001 has the status of a British Standard ICS 61.060 ? Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+
2、00:00 2006, Uncontrolled Copy, (c) BSI BS EN 13516:2002 This British Standard, having been prepared under the direction of the Materials and Chemicals Sector Policy and Strategy Committee, was published under the authority of the Standards Policy and Strategy Committee on 5 March 2002 BSI 12 May 200
3、4 ISBN 0 580 39208 2 National foreword This British Standard is the official English language version of EN 13516:2001, including Corrigendum December 2003. The UK participation in its preparation was entrusted to Technical Committee TCI/69, Footwear and leather, which has the responsibility to: A l
4、ist of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Stand
5、ards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard
6、 does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments an
7、d promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 15 and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No.
8、 DateComments 15116 Corrigendum No. 1 12 May 2004Changes to subclauses 4.3.10, 6.1.2, 6.2.1.6 and 7.1 Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13516 December 2001 ICS 61.060Incorpor
9、ating Corrigendum December 2003 English version Footwear Test methods for uppers, lining and insocks Colour fastness to rubbing Chaussures Mthodes dessai des tiges, de la doublure et des garnitures intrieures Stabilit de la couleur au frottement Schuhe Prfverfahren fr Schfte, Futter und Deckbrandsoh
10、len Farbechtheit bei Abrieb This European Standard was approved by CEN on 16 November 2001. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date
11、lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the resp
12、onsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Neth
13、erlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Management Centre: rue de Stassart, 36 B-1050 Brussels 2001 CENAll rights of exploitation in any form and by any means re
14、served worldwide for CEN national Members. Ref. No. EN 13516:2001 E Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:2001 (E) 2 Contents page Foreword3 1 Scope 4 2 Normative references4 3 Terms and definitions .4 4 Apparatus and mate
15、rial.5 4.1 Method A.5 4.2 Method B.6 4.3 Method C.7 5 Sampling and conditioning.7 5.1 Method A.7 5.2 Method B.8 5.3 Method C.8 6 Test method9 6.1 Principle9 6.1.1 Methods A and B9 6.1.2 Method C.9 6.2 Procedure .9 6.2.1 Method A.9 6.2.2 Method B.11 6.2.3 Method C.12 7 Test report13 7.1 Methods A and
16、 B13 7.2 Method C.13 Annex A .14 A.1 Summary of test conditions normally used for method B 14 A.2 Drying of pads and test specimens.14 A.3 Avoiding thermal damage.14 Bibliography15 Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:200
17、1 (E) 3 Foreword This European Standard has been prepared by Technical Committee CEN/TC 309 “Footwear“, the secretariat of which is held by AENOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by J
18、une 2002, and conflicting national standards shall be withdrawn at the latest by June 2002. Method A of this draft European Standard is based on the IULTCS/IUF 450 method (ISO 11640:1993 “Leather; tests for colour fastness; colour fastness to cycles of to-and-fro rubbing“), and method C is based on
19、the IULTCS/IUF 426 method (ISO 11641:1993 “ Leather; tests for colour fastness; colour fastness to perspiration“). Annex A is informative. This standard includes a Bibliography. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bou
20、nd to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10
21、GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:2001 (E) 4 1 Scope 1.1 This standard specifies two test methods (method A and method B) for assessing the degree of damage (marring) and transfer of a materials surface colour during mild dry or wet abrasion. The methods are applicable to all footw
22、ear upper, lining and insock irrespective of the material, in order to assess the suitability for the end use. 1.2 This standard also specifies a method (method C) for determining the likelihood of colour bleeding from materials and components such as sewing threads and shoe laces due to the action
23、of water and artificial perspiration solutions, in order to assess the suitability for the end use. 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the text
24、, and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references, the latest edition of the publication referred to appli
25、es (including amendments). EN 12222, Footwear - Standard atmospheres for conditioning and testing of footwear and components for footwear. EN ISO 105-A01, Textiles - Tests for colour fastness - Part A01: General principles of testing (ISO 105-A01:1994). EN 20105-A02, Textiles - Tests for colour fast
26、ness - Part A02: Grey scale for assessing change in colour (ISO 105- A02:1993). EN 20105-A03, Textiles - Tests for colour fastness - Part A03: Grey scale for assessing staining (ISO 105- A03:1993). EN ISO 3696, Water for analytical laboratory use - Specification and test methods (ISO 3696:1987). ISO
27、 105-F10, Textiles - Tests for colour fastness - Part F10: Specification for adjacent fabric: Multifibre. 3 Terms and definitions For the purposes of this European Standard, the following terms and definitions apply. 3.1 colour fastness to rubbing resistance of a material to damage (marring) and tra
28、nsfer of the materials surface colour during mild dry or wet abrasion 3.2 perspiration fastness resistance of a material to colour bleed when exposed to an artificial perspiration solution 3.3 thick leather leather with a thickness greater than 2 mm Licensed Copy: sheffieldun sheffieldun, na, Sun Oc
29、t 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:2001 (E) 5 4 Apparatus and material The following apparatus and material shall be used: 4.1 Method A 4.1.1 Test machine with the following: 4.1.1.1 Flat horizontal metal platform of minimum dimensions 80 mm 25 mm. 4.1.1.2 Means of mov
30、ing the platform in a direction parallel to its 80 mm edges through distance of 35 mm 2 mm and back again at a rate of 40 cycles/min 2 cycles/min. 4.1.1.3 Pair of clamps positioned at the ends of the platform at 90 to the 80 mm edges and which are designed to clamp the test specimen against the plat
31、form. The clamp faces shall be a minimum distance of 80 mm apart. 4.1.1.4 Means of moving the clamps apart so that the test specimen is extended linearly by an amount adjustable up to 20 %. 4.1.1.5 Rubbing finger with a flat horizontal lower surface capable of holding a square felt pad (4.1.2). For
32、machines with a platform wider than 25 mm the relative position of the rubbing finger shall be adjustable across the width of the platform. 4.1.1.6 Means of holding a square felt pad (4.1.2) on the lower surface of the finger. 4.1.1.7 Means of applying a downward force of 4,9 N 0,1 N and 9,8 N 0,2 N
33、 to the rubbing finger. 4.1.1.8 Means of counting the number of cycles traversed by the platform. 4.1.2 Square pads of scoured pure wool felt with the following requirements: 4.1.2.1 Sides of length 15 mm 1 mm. 4.1.2.2 Mass per unit area of 1750 g/m2 100 g/m2 and thickness 5,5 mm 0,5 mm when measure
34、d using a dial gauge exerting a downward pressure of 49 kPa 5 kPa on a measuring foot diameter of 10 mm 1 mm. 4.1.2.3 The pH of an aqueous extract, made by shaking 5 g of ground felt in 100 ml of distilled or deionized water complying with EN ISO 3696 in a polyethylene bottle and leaving for 2 h, be
35、tween 6 and 7. 4.1.3 Grey scales for assessing change in colour and staining with half step ratings conforming to EN 20105-A02 and EN 20105-A03 4.1.4 Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the assessment can be carried out in daylight from the nort
36、h, when the test is carried out in the northern hemisphere, or daylight from the south when testing in the southern hemisphere. 4.1.5 Distilled or de-mineralized water complying with grade 3 of EN ISO 3696. 4.1.6 Synthetic perspiration solution containing per litre of solution; - Sodium chloride, 5,
37、0 g per litre of solution, g/cm3. - Ammonia solution, density 0,880 g/cm3, 6,0 cm3. 4.1.7 White spirit, general purpose reagent grade. Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:2001 (E) 6 4.2 Method B 4.2.1 Test machine with t
38、he following: 4.2.1.1 Rigid horizontal platform (preferably metal) capable of clamping the test specimen. 4.2.1.2 Vertical rotating spindle capable of holding the circular felt pad. 4.2.1.3 Means of rotating the felt pad at a speed of 15,6 rad/s 0,5 rad/s1) . 4.2.1.4 Means of loading the rotating fe
39、lt pad with a force of either 24,5 N 0,5 N and 7,1 N 0,2 N. 4.2.1.5 Means of counting the number of revolutions of the felt pad. 4.2.2 Circular pads of scoured pure wool felt with central holes, with the following requirements: a) Outside diameter 25 mm 1 mm, bore diameter 3 mm 0,5 mm. b) Thickness,
40、 to be measured by one of the following methods: Thickness Downward pressure/presser foot size Specimen 6,5 0,5 49 kPa 5 kPa/10 mm 1 mm Cut pads or uncut sheet material 5,0 0,5 2,0 kPa 0,2 kPa/19 mm 10 mm Cut pads c) Density 190 kg/m3 20 kg/m3. 4.2.3 Grey scales for assessing the change in colour an
41、d degree of staining complying with EN 20105-A02 and EN 20105-A03 respectively. 4.2.4 Metal plate approximately 75 mm 65 mm and thickness 5 mm with a hole diameter 25 mm through its centre for use in the wetting from the back with organic solvents test described in 6.2.2.6. 4.2.5 Polished aluminium
42、disc (diameter approximately 50 mm and thickness approximately 12 mm) to help cool the test specimen in dry rub tests. 4.2.6 Balance, capable of weighing masses up to 5 g to an accuracy of 10 mg. 4.2.7 Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the ass
43、essment can be carried out in daylight from the north, when the test is carried out in the northern hemisphere, or daylight from the south when testing in the southern hemisphere. 4.2.8 Distilled or deionised water complying with grade 3 of EN ISO 3696 for the wet rub test described in 6.2.2.3. 4.2.
44、9 Synthetic perspiration solution, for the perspiration rub test described in 6.2.2.4, consisting of: - Sodium chloride, 5 g per litre of solution, g/cm3. - Ammonia solution, density 0,880 g/cm3, 6,0 cm3. 4.2.10 White spirit for the spirit rub test described in 6.2.2.5. 4.2.11 Organic solvents (as u
45、sed for solvent activated stiffeners) for the wetting from the back with organic solvents test described in 6.2.2.6. 1) 1 rad 0,16 rev. Licensed Copy: sheffieldun sheffieldun, na, Sun Oct 29 15:41:10 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN 13516:2001 (E) 7 4.3 Method C 4.3.1 Petri dish large e
46、nough to accommodate a glass plate (4.3.2) for each test specimen assembly. 4.3.2 Glass plate of length at least 110 mm and width at least 55 mm with a mass of 100 g 2 g for each test specimen assembly. 4.3.3 Rectangular pieces of multifibre fabric type DW as specified in ISO 105-F10 of dimensions 1
47、00 mm 5 mm 50 mm 2 mm. 4.3.4 Oven maintained at a temperature of 37 C 2 C. 4.3.5 Grey scales for assessing change in colour and staining with half steps as described in EN 20105-A02 and EN 20105-A03. 4.3.6 Assessment cabinet with artificial lighting as specified in EN ISO 105-A01. Alternatively, the
48、 assessment can be carried out in daylight from the north, when the test is carried out in the northern hemisphere, or daylight from the south when testing in the southern hemisphere. 4.3.7 Balance capable of measuring mass up to 100 g to the nearest 0,1 g for testing yarns or loose fibres. 4.3.8 Di
49、stilled or de-mineralized water complying with grade 3 of EN ISO 3696. 4.3.9 Alkaline perspiration solution containing, per litre of solution; - l-histidine monohydrochloride monohydrate: 5,00 g. - Sodium chloride: 5,00 g. - Disodium hydrogen orthophosphate dihydrate: 2,50 g. After preparation, the solution is brought to pH 8 with 0,1 M sodium hydroxide solution. Store the solution at 4 C 1 C. If the solution is more than one