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1、BRITISH STANDARD BS EN ISO 1516:2002 BS 2000-491: 2002 Incorporating Corrigendum No. 1 Method of test for petroleum and its products BS 2000-491: Determination of flash/no flash Closed cup equilibrium method (Identical with IP 491-2003) The European Standard EN ISO 1516:2002 has the status of a Brit
2、ish Standard ICS 75.080; 87.040 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 1516:2002 This British Standard, having been prepared under the direction of the
3、 Materials and Chemicals Sector Policy and Strategy Committee, was published under the authority of the Standards Policy and Strategy Committee on 7 May 2002 Institute of Petroleum and BSI 30 May 2002 ISBN 0 580 39224 4 National foreword This British Standard is the official English language version
4、 of EN ISO 1516:2002. It is identical with ISO 1516:2002. The UK participation in its preparation was entrusted to Technical Committee PTI/13, Petroleum testing and terminology, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its s
5、ecretary. The Institute of Petroleum publishes and sells all parts of BS 2000, and all BS EN petroleum test methods that would be part of BS 2000, both in its annual publication “Standard methods for analysis and testing of petroleum and related products and British Standard 2000 Parts” and individu
6、ally. Further information is available from: The Institute of Petroleum, 61 New Cavendish Street, London, W1G 7AR. Tel: 020 7467 7100. Fax: 020 7255 1472. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BS
7、I Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are respon
8、sible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible International/European committee any enquiries on the interpretation, or proposals for change, and keep
9、the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii to v, a blank page, pages 1 t
10、o 9, the Annex ZA page, an inside back cover and a back cover. The BSI copyright date displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments 13951 Corrigendum No. 1 30 May 2002Incorporating the Annex ZA page Licensed Copy: sh
11、effieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1516 March 2002 ICS 75.080; 87.040 English version Determination of flash/no flash - Closed cup equilibrium method (ISO 1516:2002) Essai de point declair
12、 de type passe/ne passe pas - Mthode lquilibre en vase clos (ISO 1516:2002) Flammpunktbestimmung - Ja/Nein-Verfahren - Gleichgewichtsverfahren mit geschlossenem Tiegel (ISO 1516:2002) This European Standard was approved by CEN on 1 March 2002. CEN members are bound to comply with the CEN/CENELEC Int
13、ernal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Management Centre or to any CEN member
14、. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official versions. CEN members are
15、 the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATI
16、ON EUROPISCHES KOMITEE FR NORMUNG Management Centre: rue de Stassart, 36 B-1050 Brussels 2002 CENAll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1516:2002 E Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00
17、2006, Uncontrolled Copy, (c) BSI CORRECTED 2002-05-08 Foreword This document (ISO 1516:2002) has been prepared by Technical Committee ISO/TC 28 “Petroleum products and lubricants“ in collaboration with Technical Committee CEN/TC 19 “Petroleum products, lubricants and related products“, the secretari
18、at of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2002, and conflicting national standards shall be withdrawn at the latest by September 2002. According to the
19、CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spa
20、in, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard ISO 1516:2002 has been approved by CEN as a European Standard without any modifications. NOTE Normative references to International Standards are listed in annex ZA (normative). EN ISO 1516:2002
21、 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Reference number ISO 1516:2002(E) INTERNATIONAL STANDARD ISO 1516 Third edition 2002-03-01 Determination of flash/no flash Closed cup equilibrium method Essai de point dclair de type passe/ne
22、passe pas Mthode lquilibre en vase clos EN ISO 1516:2002 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ii EN ISO 1516:2002 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 1516:
23、2002(E) iii Contents Page Foreword.iv Introduction.v 1 Scope1 2 Normative references1 3 Term and definition .2 4 Principle2 5 Chemicals and materials.2 6 Apparatus.2 7 Apparatus preparation3 8 Sampling.4 9 Sample handling4 10 Test temperature5 11 Procedure.5 12 Expression of results7 13 Precision.7
24、14 Test report7 Annex A (informative) Precision data from ISO 15238 Bibliography9 EN ISO 1516:2002 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 1516:2002(E) iv Foreword ISO (the International Organization for Standardization) is a wor
25、ldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on
26、 that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted
27、in accordance with the rules given in the ISO/IEC Directives, Part 3. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standar
28、d requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this International Standard may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 1516 was
29、prepared jointly by Technical Committees ISO/TC 28, Petroleum products and lubricants and ISO/TC 35, Paints and varnishes. This third edition cancels and replaces the second edition (ISO 1516:1981), which has been technically revised. Annex A of this International Standard is for information only. E
30、N ISO 1516:2002 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 1516:2002(E) v Introduction This International Standard describes one of two closed cup equilibrium methods for carrying out a flash/no flash test for paints, varnishes, pet
31、roleum and related products, and it should be read in conjunction with the second equilibrium method, ISO 3680 (2 in the bibliography), when selecting a method. The determination of the flash point using the same equipment is described in ISO 1523. This test method does not determine the flash point
32、 of the product under test, but merely its behaviour at the selected equilibrium temperature as may be required to comply with laws or regulations relating to the storage, transport and use of flammable products. For this purpose, it is unnecessary to determine the exact flash point, but it is neces
33、sary to determine whether or not flashing occurs at a given temperature. By the procedure specified, differences between test apparatus of various standard designs are minimized by ensuring that the test is carried out only when the product under test and the air/vapour mixture above it in the test
34、vessel are considered to be in temperature equilibrium. EN ISO 1516:2002 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI blank Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI INTENRA
35、TIONALTS ANDA DRIS:6151 O2002(E) I SO 2002 All irthgs ersedevr 1 Determination of flash/no flash Closed cup equilibrium method WARNING The use of this International Standard may involve hazardous materials, operations and equipment. This International Standard does not purport to address all of the
36、safety problems associated with its use. It is the responsibility of the user of this International Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1 Scope This International Standard specifies a method to determin
37、e if paints, varnishes, paint binders, solvents, petroleum or related products, when maintained at a selected equilibrium temperature and under the conditions of the test, give off sufficient flammable vapour to cause ignition on application of an external source of flame applied in a standard manne
38、r. This International Standard is not applicable to water-borne paints which may, however, be tested using ISO 3680 (2 in the bibliography). The method is suitable for use over the temperature range 30 C to 110 C, depending on the use of different apparatus listed in Table 1. The interpretation of r
39、esults obtained from solvent mixtures containing halogenated hydrocarbons should be considered with caution, as these mixtures can give anomalous results. 2 Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this
40、International Standard. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreements based on this International Standard are encouraged to investigate the possibility of applying the most recent editions of the normative doc
41、uments indicated below. For undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC maintain registers of currently valid International Standards. ISO 1513:1992, Paints and varnishes Examination and preparation of samples for testing ISO 1523:2002
42、, Determination of flash point Closed cup equilibrium method ISO 2719:1), Determination of flash point Pensky-Martens closed cup method ISO 3170:1988, Petroleum liquids Manual sampling ISO 3171:1988, Petroleum liquids Automatic pipeline sampling ISO 13736:1997, Petroleum products and other liquids D
43、etermination of flash point Abel closed cup method ISO 15528:2000, Paints, varnishes and raw materials for paints and varnishes Sampling 1) To be published. (Revision of ISO 2719:1988) EN ISO 1516:2002 1 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 03:02:00 GMT+00:00 2006, Uncontrolled Cop
44、y, (c) BSI IS:6151 O2002(E) 2 ISO 2002 Allir thgser se devr ASTM D56-00, Standard Test Method for Flash Point by Tag Closed Tester DIN 51755:1974, Testing of mineral oils and other combustible liquids; determination of flash point by the closed tester according to Abel-Pensky 3 Term and definition F
45、or the purposes of this International Standard, wherein ignition source is recognized as being a flame, the following term and definition applies. 3.1 flash point lowest temperature of the test portion, corrected to a barometric pressure of 101,3 kPa, at which application of an ignition source cause
46、s the vapour of the test portion to ignite and the flame to propagate across the surface of the liquid under the specified conditions of test 4 Principle The test portion is placed in a suitably designed closed cup mounted in a thermostatically controlled bath. After the test portion has been mainta
47、ined at the selected equilibrium temperature conditions for at least 10 min, an ignition trial is carried out by directing a small flame into the test cup. Whether or not the test flame causes the vapour above the test portion to ignite, is recorded. 5 Chemicals and materials 5.1 Cleaning solvent, f
48、or removal of traces of the previous test portion from the test cup and cover. NOTE The choice of solvent will depend upon the previous material tested, and the tenacity of the residue. Low volatility aromatic (benzene-free) solvents may be used to remove traces of oil, and mixed solvents such as to
49、luene-acetone-methanol may be effective for the removal of gum-type deposits. 5.2 Verification liquids, see ISO 1523. 6 Apparatus 6.1 Test cup and lid: a closed cup with, where specified, an internal level indicator, and lid, as specified in the standards listed in Table 1. The test cup shall be fitted with a tightly fitting cover which carries an opening slide and an ignition device capable, when the slide is open, of positioning an ignition flame, with a diameter of between 3 mm and 4 mm, at the approximate centre of th