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1、BRITISH STANDARD CONFIRMED FEBRUARY 1998 BS EN ISO 1513:1995 BS 3900-A2: 1993 Incorporating Amendment No. 1 Paints and varnishes Examination and preparation of samples for testing The European Standard EN ISO 1513:1994 has the status of a British Standard NOTEIt is recommended that this Part be read
2、 in conjunction with BS 3900-0, issued separately. UDC 667.61:620.11 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 1513:1995 This British Standard, having been prepared under the direction of the Pigments, Paints and Varnishes St
3、andards Policy Committee, was published under the authority of the Standards Board and comes into effect on 15 March 1993 BSI 09-1999 First published February 1970 Second edition February 1983 Third edition March 1993 The following BSI references relate to the work on this standard: Committee refere
4、nce PVC/10 Draft for comment 91/56748 DC ISBN 0 580 22058 3 Committees responsible for this British Standard The preparation of this British Standard was entrusted by the Pigments, Paints and Varnishes Standards Policy Committee (PVC/-) to Technical Committee PVC/10, upon which the following bodies
5、were represented: European Resin Manufacturers Association Health and Safety Executive Institute of Metal Finishing Ministry of Defence National Centre of Tribology Oil and Colour Chemists Association Paint Research Association Paintmakers Association of Great Britain Ltd. Titanium Pigment Manufactu
6、rers Technical Committee Amendments issued since publication Amd. No.DateComments 8331February 1995 Indicated by a sideline in the margin Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 1513:1995 BSI 09-1999i Contents Page Committe
7、es responsibleInside front cover National forewordii Foreword2 Text of EN ISO 15133 List of referencesInside back cover Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 1513:1995 ii BSI 09-1999 National foreword This Part of BS 3900
8、 has been prepared under the direction of the Pigments, Paints and Varnishes Standards Policy Committee. It is identical with ISO 1513:1992 Paints and varnishes Examination and preparation of samples for testing, published by the International Organization for Standardization (ISO). In 1994 the Euro
9、pean Committee for Standardization (CEN) accepted ISO 1513:1992 and its Technical Corrigendum 1:1994 as European Standard EN ISO 1513:1994. This edition supersedes BS 3900-A2:1983, which is withdrawn. The main difference between BS 3900-A2:1983 and this standard is that discarding samples with surfa
10、ce skin is now recommended. The Technical Committee has reviewed the provisions of ISO 565, to which normative reference is made in the text, and has decided that they are acceptable for use in conjunction with this standard. A related British Standard to ISO 565 is BS 410:1986 Specification for tes
11、t sieves. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Cross-references International
12、StandardCorresponding British Standard ISO 1512:1991 BS 3900 Methods of test for paints Part A1:1992 Sampling (Identical) Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, the EN ISO title page, pages 2 to 6, an inside back cover and a back cover. This st
13、andard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE
14、 EUROPISCHE NORM EN ISO 1513 August 1994 UDC 667.61:620.11Supersedes EN 21513:1991 Descriptors: Paints, varnishes, tests, examination, samples, test specimens, specimen preparation English version Paints and varnishes Examination and preparation of samples for testing (ISO 1513:1992) Peintures et ve
15、rnis Examen et prparation des chantillons pour essais (ISO 1513:1992) Lacke und Anstrichstoffe Vorprfung und Vorbereitung von Proben fr weitere Prfungen (ISO 1513:1992) This European Standard was approved by CEN on 1994-08-22. CEN members are bound to comply with the CEN/CENELEC Internal Regulations
16、 which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. The European
17、Standards exist in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national
18、standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung
19、 Central Secretariat: rue de Stassart 36, B-1050 Brussels 1994 Copyright reserved to CEN members Ref. No. EN ISO 1513:1994 E Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 1513:1994 2 BSI 09-1999 Foreword This European Standard has b
20、een taken over by the Technical Committee CEN/TC 139, Paints and varnishes, from the work of ISO/TC 35, Paints and varnishes, of the International Organization for Standardization (ISO). This European Standard replaces EN 21513:1991. This European Standard shall be given the status of a national sta
21、ndard, either by publication of an identical text or by endorsement, at the latest by February 1995, and conflicting national standards shall be withdrawn at the latest by February 1995. According to the CEN/CENELEC Internal Regulations, the following countries are bound to implement this European S
22、tandard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. Contents Page Foreword2 1Scope3 2Normative references3 3Sample container3 4Preliminary procedure for fluid products
23、 such as varnishes, emulsions, thinners, etc.3 5Preliminary procedure for fluid products such as paints4 6Preliminary procedure for viscous products such as putties, mastics, etc.4 7Preliminary procedure for products in powder form4 8Blending and reduction of a series of samples5 9Labelling of sampl
24、e containers5 10Preliminary examination report5 Annex ZA (normative) Normative references to international publications with their relevant European publications6 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 1513:1994 BSI 09-19993
25、1 Scope This International Standard is one of a series of standards dealing with the sampling and testing of paints, varnishes and related products. This International Standard specifies both the procedure for preliminary examination of a single sample as received for testing, and the procedure for
26、preparing a test sample by blending and reduction of a series of samples representative of a consignment or bulk of paint, varnish or related product, the samples of the product to be tested having been taken in accordance with ISO 1512. 2 Normative references The following standards contain provisi
27、ons which, through reference in this text, constitute provisions of this International Standard. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this International Standard are encouraged to investigate the poss
28、ibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 565:1990, Test sieves Metal wire cloth, perforated metal plate and electroformed sheet Nominal sizes of openings. ISO 1512:1991, Pa
29、ints and varnishes Sampling of products in liquid or paste form. 3 Sample container 3.1 Condition of container Record any defects in the sample container or any visible leakage. If it is possible that the contents have been affected, the sample shall be rejected. 3.2 Opening of a container WARNING S
30、ome paints and related products (such as paint removers) are prone to develop gas or vapour pressure during storage. Care, appropriate to the situation, shall be taken in opening containers, particularly if bulging of the lid or the bottom of the container is observed. If such phenomena occur, they
31、shall be noted in the report (clause 10). Remove all packing materials and other debris from the outer surface of the container, particularly around the closure. Open the container carefully, taking care not to disturb the contents. 4 Preliminary procedure for fluid products such as varnishes, emuls
32、ions, thinners, etc.1) 4.1 Visual examination 4.1.1 Ullage Record the approximate ullage, i.e. the air-space above the contents of the container, expressed as a percentage of the total capacity of the container. 4.1.2 Surface skin Record the presence of any surface skin and whether the skin is conti
33、nuous, hard, soft, thin or moderately or excessively thick. If skin is observed on the sample, it is preferable to discard the sample. If this is impractical, detach the skin as completely as possible from the sides of the container and remove it, if necessary by straining. Record the ease of remova
34、l. For analytical control purposes, where skin is present, it may be necessary to disperse the skin and include it in the sample for testing. 4.1.3 Consistency Record whether the sample is thixotropic or whether gelling has taken place, taking care not to confuse gelling and thixotropy. NOTE 1Both t
35、hixotropic and gelled varnishes have a jelly-like consistency but, whereas the consistency of the former is markedly reduced by stirring or shaking, the consistency of a gelled varnish cannot be reduced in this way. 4.1.4 Separation into layers Record any separation of the sample into layers, for ex
36、ample water and oily or resinous matter. 4.1.5 Visible impurities If there are any visible impurities, record their presence and remove them if possible. 4.1.6 Sediment If there is any appreciable sediment, record its presence and appearance. 4.1.7 Clarity and colour In the case of varnishes, thinne
37、rs, catalyst solutions, etc., record the clarity and colour of the sample. 4.2 Mixing Thoroughly stir the sample and incorporate any slight sediment. 1) These correspond to type A and B products in ISO 1512. Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 20 02:57:30 GMT+00:00 2006, Uncontrolled
38、 Copy, (c) BSI EN ISO 1513:1994 4 BSI 09-1999 5 Preliminary procedure for fluid products such as paints2) 5.1 Visual examination 5.1.1 Ullage Record the approximate ullage, i.e. the air-space above the contents of the container, expressed as a percentage of the total capacity of the container. 5.1.2
39、 Surface skin Record the presence of any surface skin and whether the skin is continuous, hard, soft, thin or moderately or excessively thick. If skin is observed on the sample, it is preferable to discard the sample. If this is impractical, detach the skin as completely as possible from the sides o
40、f the container and remove it, if necessary by straining. Record the ease of removal. For analytical control purposes, where skin is present, it may be necessary to disperse the skin and include it in the sample for testing. 5.1.3 Consistency Record whether the sample is thixotropic or whether gelli
41、ng has taken place, taking care not to confuse gelling and thixotropy. NOTE 2Both thixotropic and gelled paints have a jelly-like consistency but, whereas the consistency of the former is markedly reduced by stirring or shaking, the consistency of a gelled paint cannot be reduced in this way. 5.1.4
42、Separation into layers Record any separation of the sample into layers. 5.1.5 Settling Record the type of settling, for example soft, hard or hard-dry. If the settling is hard and appears dry and crumbly inside a lump when cut with a clean palette knife, describe it as “hard-dry”. 5.1.6 Extraneous m
43、atter Record the presence of any extraneous matter in the paint and remove it as carefully as possible. 5.2 Mixing 5.2.1 Limitations Samples which have gelled or show hard-dry settling (see 5.1.3 and 5.1.5) cannot be effectively reincorporated and shall therefore not be used for testing purposes. 5.
44、2.2 General During all the operations specified in 5.2.3 to 5.2.5, take care to ensure minimum loss of solvent. To this end, carry out all the operations as rapidly as practicable, consistent with satisfactory mixing. 5.2.3 Removal of skin If the original sample contained skin, detach and remove any
45、 remnants by straining the incorporated sample, under its own weight, through a sieve complying with ISO 565, of nominal aperture 125 4m, unless otherwise specified. 5.2.4 If no hard settling has occurred Mix the sample thoroughly, even if there is no perceptible settling. NOTE 3If the sample is sma
46、ll enough, a palette knife is suitable, but for a larger sample a stouter stirrer is needed. Firmly replace the lid of the container and thoroughly shake the contents, inverting the container while this is being done. Alternately stir and shake the container in this way until the contents are comple
47、tely homogeneous. NOTE 4As an added precaution, it is recommended that the mixing should be completed by pouring the contents into a clean container and back again several times. At all times during the sample preparation, avoid, as far as possible, entrainment of air. The sample shall be free from
48、air bubbles before use. 5.2.5 If hard settling has occurred If it is required to complete the examination of a sample in which hard settling has occurred (but not hard-dry settling, see 5.2.1), proceed as follows. Pour all the fluid medium into a clean container. Remove the settled pigment from the
49、bottom of the original container with a palette knife and mix thoroughly. When a uniform consistency has been achieved, return the fluid medium to the original container, a small portion at a time, carefully incorporating each addition before the next is made. Complete the reincorporation by pouring from one container to the other several time (see 5.2.4). The sample shall be free from air bubbles before use. 6 Preliminary procedure for viscous products such as putties, mastics, etc.3) Examine these products in general as for paints under clause 5