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1、BRITISH STANDARD BS EN ISO 5667-13:1998 BS 6068-6.13: 1998 Incorporating Corrigendum No. 1 and No. 2 Water quality Sampling Part 13: Guidance on sampling of sludges from sewage and water treatment works The European Standard EN ISO 5667-13:1997 has the status of a British Standard ICS 13.060.30 Lice
2、nsed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 5667-13:1998 This British Standard, having been prepared under the direction of the Health and Environment Sector Board, was published under the authority of the Standards Board and comes
3、 into effect on 15 April 1998 BS1 05-1999 ISBN 0 580 29279 7 Amendments issued since publication Amd. No.DateComments 10043 Corr. No. 1 May 1998correction to front and back covers 10228 Corr. No. 2 January 1999 Addition of annex ZA Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+
4、00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 5667-13:1998 BSI 05-1999i Contents Page National forewordii Foreword2 Forewordiii Text of ISO 5667-131 Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 5667-13:1998 ii BSI 05-1999 Nat
5、ional foreword This British Standard is the English language version of EN ISO 5667-13:1997. It is identical with ISO 5667-13:1997. The UK participation in its preparation was entrusted by Technical Committee EH/3, Water quality, to Subcommittee EH/3/6, Sampling, which has the responsibility to: aid
6、 enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. A list of organizati
7、ons represented on this committee can be obtained on request to its secretary. BS EN ISO 5667-13 is one of a series of standards on water quality, others of which have been, or will be, published as Sections of BS 6068. This standard has therefore been given the secondary identifier BS 6068-6.13. Th
8、e various Sections of BS 6068 are comprised within Parts 1 to 7, which, together with Part 0, are listed below. Part 0: Introduction; Part 1: Glossary; Part 2: Physical, chemical and biochemical methods; Part 3: Radiological methods; Part 4: Microbiological methods; Part 5: Biological methods; Part
9、6: Sampling; Part 7: Precision and accuracy. Cross-references Attention is drawn to the fact that CEN and CENELEC Standards normally include an annex which lists normative references to international publications with their corresponding European publications. The British Standards which implement t
10、hese international or European publications may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessa
11、ry provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, the EN I
12、SO title page, page 2, the ISO title page, pages ii to iv, pages 1 to 14, and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover. Licensed Copy: sheffieldun sheffieldun, n
13、a, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 5667-13 December 1997 ICS 13.030.20 Descriptors: See IS0 document English version Water quality Sampling Part 13: Guidance on sampling of sludges from sewage and water treatment
14、 works (ISO 5667-13:1997) Qualit de leau Echantillonnage Partie 13: Guide pour lchantillonnage de boues provenant dinstallations de traitement de leau et des eaux uses (ISO 5667-13:1997) This European Standard was approved by CEN on 20 December 1997. CEN members are bound to comply with the CEN/CENE
15、LEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any C
16、EN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN
17、members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Nor
18、malisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1997 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 5667-13:1997 E Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49
19、:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 5667-13:1997 BSI 05-1999 2 Foreword The text of the International Standard ISO 5667-13:1997 has been prepared by Technical Committee ISO/TC 147 “Water quality” in collaboration with Technical Committee CEN/TC 308 “Characterization of sludges”, th
20、e secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 1998, and conflicting national standards shall be withdrawn at the latest by June 1998. According to t
21、he CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain,
22、Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard ISO 5667-13:1997 was approved by CEN as a European Standard without any modification. NOTENormative references to International Standards are listed in Annex ZA (normative). Licensed Copy: sheffield
23、un sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 5667-13:1997 ii BSI 05-1999 Contents Page Forewordiii Introduction 1 1Scope1 2Normative references1 3De
24、finitions1 4Sampling equipment2 5Sampling procedure3 6Storage, preservation and handling7 7Safety9 8Reporting10 Annex A (informative) Vacuum sampling devices11 Annex B (informative) Apparatus for sampling from pipes under pressure12 Annex C (informative) Bibliography13 Annex ZA (normative) Normative
25、 references to international publications with their relevant European publications14 Figure 1 Typical riffle box9 Figure A.1 Suggested apparatus for the sampling of thick liquid sludge under vacuum12 Figure B.1 Recommended valve arrangement for sampling liquid sludge under pressure13 Descriptors: W
26、ater, quality, sewage, sludges, water pollution, sampling, sampling equipment, rules (instructions). Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 5667-13:1997 BSI 05-1999iii Foreword ISO (the International Organization for Standard
27、ization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to
28、be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International
29、 Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard ISO 5667-13 was prepared by Technical Committee ISO/TC 147, Water qua
30、lity, Subcommittee SC 6, Sampling (general method). International Standard ISO 5667 consists of the following parts, under the general title Water quality Sampling Part 1: Guidance on the design of sampling programmes; Part 2: Guidance on sampling techniques; Part 3: Guidance on the preservation and
31、 handling of samples; Part 4: Guidance on sampling from lakes, natural and man-made; Part 5: Guidance on sampling of drinking water and water used for food and beverage processing; Part 6: Guidance on sampling of rivers and streams; Part 7: Guidance on sampling of water and steam in boiler plants; P
32、art 8: Guidance on the sampling of wet deposition; Part 9: Guidance on sampling from marine waters; Part 10: Guidance on sampling of waste waters; Part 11: Guidance on sampling of groundwaters; Part 12: Guidance on sampling of bottom sediments; Part 13: Guidance on sampling of sludges from sewage an
33、d water treatment works; Part 14: Guidance on quality assurance of environmental water sampling and handling; Part 16: Guidance on biotesting of samples. Annex A, Annex B and Annex C of this part of ISO 5667 are for information only. Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GM
34、T+00:00 2006, Uncontrolled Copy, (c) BSI iv blank Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:00 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 5667-13:1997 BSI 05-19991 Introduction This part of ISO 5667 should be read in conjunction with ISO 5667-1, ISO 5567-2 and ISO 5667-3. T
35、he general terminology used is in accordance with the various parts of ISO 6107. Sampling and the determination of the physical and chemical properties of sludges and related solids are normally carried out for a specific purpose. The sampling methods given are suitable for general use but do not ex
36、clude modification in the light of any special factor known to the analyst receiving the samples or any operational reason dictating the need for sampling. The importance of using a valid sampling technique cannot be overemphasized if the subsequent analysis is to be worthwhile. It is important that
37、 the personnel taking and analysing the sample be fully aware of its nature and the purpose for which the analysis is required before embarking on any work programme. Full cooperation with the laboratory that will be analysing the samples ensures that the most effective application of the sampling o
38、ccasion can be made. For example, the use of method-specific sample preservation techniques will assist in the accurate determination of results. 1 Scope This part of ISO 5667 gives guidance on the sampling of sludges from wastewater treatment works, water treatment works and industrial processes. I
39、t is applicable to all types of sludge arising from these works and also to sludges of similar characteristics, for example septic tank sludges. Guidance is also given on the design of sampling programmes and techniques for the collection of samples. This part of ISO 5667 is applicable to sampling m
40、otivated by different objectives, some of which are to: provide data for the operation of activated sludge plants; provide data for the operation of sludge treatment facilities; determine the concentration of pollutants in wastewater sludges for disposal to landfill; test whether prescribed substanc
41、e limits are contravened when sludge is used in agriculture; provide information on process control in potable and wastewater treatment, including: a) addition or withdrawal of solids; b) addition or withdrawal of liquid; provide information for legally enforceable aspects of the disposal of sewage
42、and waterworks sludges; facilitate special investigations into the performance of new equipment and processes; optimize costs; for example for the transport of sludges for treatment and/or disposal. NOTEWhen designing a sludge sampling programme, it is essential that the objectives of the study be k
43、ept in mind, so that the information gained corresponds to that required. In addition, the data should not be distorted by the use of inappropriate techniques, such as inadequate storage temperatures or the sampling of unrepresentative parts of a treatment plant. 2 Normative references The following
44、 standards contain provisions which, through reference in this text, constitute provisions of this part of ISO 5667. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO 5667 are encouraged to invest
45、igate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 5667-2:1991, Water quality Sampling Part 2: Guidance on sampling techniques. ISO 5667-3:1994, Water quality Sampling
46、Part 3: Guidance on the preservation and handling of samples. ISO 5667-12:1995, Water quality Sampling Part 12: Guidance on sampling of bottom sediments. ISO 5667-14:, Water quality Sampling Part 14: Guidance on quality assurance of environmental water sampling and handling1). ISO 8363:, Measurement
47、 of liquid flow in open channels General guidelines for selection of method2). ISO 10381-6:1993, Soil quality Sampling Part 6: Guidance on the collection, handling and storage of soil for the assessment of aerobic microbial processes in the laboratory. 3 Definitions For the purposes of this part of
48、ISO 5667, the following definitions apply: 3.1 grab sample discrete sample taken randomly (with regard to time and/or location) from a body of sludge Based on ISO 6107-2 1) To be published. 2) To be published. (Revision of ISO 8363:1986) Licensed Copy: sheffieldun sheffieldun, na, Sat Nov 18 01:49:0
49、0 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 5667-13:1997 2 BSI 05-1999 3.2 composite sample two or more samples or subsamples, mixed together in appropriate known proportions (either discretely or continuously), from which the average value of a desired characteristic may be obtained NOTEThe proportions are usually based on time or flow measurements. Based on ISO 6107-2 3.3 flow-related sampling samples taken at varying time intervals gover