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1、BRITISH STANDARD BS EN ISO 105-E12:1997 Incorporating Technical Corrigenda Nos. 1 and 2 Textiles Tests for colour fastness Part E12: Colour fastness to milling: Alkaline milling (ISO 105-E12:1989) The European Standard EN ISO 105-E12:1997 has the status of a British Standard ICS 59.080.01 ? Licensed
2、 Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 105-E12:1997 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and come
3、s into effect on 15 August 1997 BSI 25 February 2003 ISBN 0 580 27841 7 National foreword This British Standard is the English language version of EN ISO 105-E12:1997. It is identical with ISO 105-E12:1989, including Technical Corrigendum February 2002. It supersedes the relevant method in BS 1006:1
4、990 which is withdrawn by amendment. The UK participation in its preparation was entrusted by Technical Committee TCI/25, Chemical properties, to Subcommittee TCI/25/-/10, Colour fastness, which has the responsibility to: A list of organizations represented on this subcommittee can be obtained on re
5、quest to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI
6、 Electronic Catalogue or of British Standard Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers
7、 to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document
8、 comprises a front cover, an inside front cover, pages i and ii, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii to iv, pages 1 to 4, an inside back cover and a back cover. The BSI copyright notice displayed in this document indicates the most recent changes by amendmen
9、t. Amendments issued since publication Amd. No.DateComments 13670 Technical Corrigendum 26 July 2002Changes to Clause 2, Subclause 4.3 and Table 1 14380 Tech Corr. No. 2 25 February 2003 Corrected EN ISO foreword page Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Un
10、controlled Copy, (c) BSI BS EN ISO 105-E12:1997 BSI 25 February 2003 i Contents Page National forewordInside front cover Forewordiii Text of ISO 105-E121 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ii blank Licensed Copy: sheffieldun she
11、ffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-E12 April 1997 ICS 59.080.01 Descriptors: See ISO document English version Textiles Tests for colour fastness Part E12: Colour fastness to milling: Alkaline milli
12、ng (ISO 105-E12:1989) Textiles Essais de solidit des teintures Partie E12: Solidit des teintures au foulon: Foulon alcalin (ISO 105-E12:1989) Textilien Farbechtheitsprfungen Teil E12: Farbechtheit gegen Walken: Alkalische Walke (ISO 105-E12:1989) This European Standard was approved by CEN on 1997-03
13、-28. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained
14、 on application to the Central Secretariat or to any CEN member. The European Standards exist in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretari
15、at has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for
16、 Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1997 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 105-E12:1997 E Licensed Copy: sheffiel
17、dun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E12:1997 BSI 25 February 2003 Foreword This document (EN ISO 105-E12:1997/A1:2002) has been prepared by Technical Committee ISO/TC 38, Textiles, in collaboration with Technical Committee CEN/TC 248, Textil
18、es and textile products, the Secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2003, and conflicting national standards shall be withdrawn at the latest by M
19、ay 2003. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherla
20、nds, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 105-E12:1997/A1:2002 has been approved by CEN as EN ISO 105-E12:1997/A1:2002 without any modifications. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontr
21、olled Copy, (c) BSI Technical corrigendum 2002-02-01 Reference number ISO 105-E12:1989 Corr.1:2002 (E) Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E12:1997 ii BSI 25 February 2003 Contents Page Forewordiii 1Scope1 2Normative r
22、eferences1 3Principle1 4Apparatus and reagents1 5Test specimen2 6Procedure2 7Test report3 8Notes3 Annex ZA (normative) Normative references to international publications with their relevant European publications4 Table 1 Single-fibre adjacent fabrics2 Licensed Copy: sheffieldun sheffieldun, na, Sun
23、Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E12:1997 BSI 25 February 2003 iii Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is norma
24、lly carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in th
25、e work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for approval before their acceptance as International St
26、andards by the ISO Council. They are approved in accordance with ISO procedures requiring at least 75 % approval by the member bodies voting. International Standard ISO 105-E12 was prepared by Technical Committee ISO/TC 38, Textiles. This third edition cancels and replaces the second edition (ISO 10
27、5-E12:1987), of which it constitutes a technical revision. ISO 105 was previously published in 13 “parts”, each, designated by a letter (e.g. “Part A”), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a tw
28、o-digit serial number (e.g. “Section A01”). These sections are now being republished as separate documents, themselves designated “parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. Descriptors: Textiles, dyes, tests, chemical tests,
29、 alkali resistance tests, determination, colour fastness, alkalis. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI iv blank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105
30、-E12:1997 BSI 25 February 2003 1 1 Scope This part of ISO 105 specifies a method for determining the resistance of the colour of wool and part-wool textiles to the action of soap and sodium carbonate solutions used in alkaline milling. 2 Normative references The following standards contain provision
31、s which, through reference in this text, constitute provisions of this part of ISO 105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of apply
32、ing the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1994, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1987, Textiles Tests for colour fastness Part
33、 A02: Grey scale for assessing change in colour. ISO 105-A03:1987, Textiles Tests for colour fastness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Textiles Tests for colour fastness Part F: Standard adjacent fabrics. ISO 105-F10:1989, Textiles Tests for colour fastness Part F10: Spec
34、ification for adjacent fabric: Multifibre. 3 Principle A specimen of the textile in contact with one or two specified adjacent fabrics is milled in a jar containing steel balls and a solution of soap and sodium carbonate. The severity of the action is controlled by means of a test-control dyeing mil
35、led separately in the same way. After rinsing and drying, the change in colour of the specimen and the staining of the adjacent fabrics are assessed with the grey scales. 4 Apparatus and reagents 4.1 Suitable mechanical device (see 8.1), consisting of a water bath containing a rotatable shaft which
36、supports, radially, glass or stainless steel containers (75 mm ? 5 mm diameter ?125 mm ?10 mm high) of approximately 550 ml ?50 ml capacity, the bottom of the containers being 45 mm ?10 mm high from the centre of the shaft. The shaft/container assembly is rotated at a frequency of 40 min1 ?2 min1. T
37、he temperature of the water bath is thermostatically controlled to maintain the test solution at the prescribed temperature of 40?C?2?C. 4.2 Non-corrodible (stainless) steel balls, approximately 6 mm in diameter. 4.3 Adjacent fabrics (see ISO 105-A01:1994, subclause 8.2. Either: 4.3.1 A multifibre a
38、djacent fabric complying with ISO 105-F10. Or: 4.3.2 Two single-fibre adjacent fabrics, complying with the relevant sections of F01 to F08 of ISO 105-F:1985. One of the adjacent fabrics shall be made of the same kind of fibre as that of the textile to be tested, or that predominating in the case of
39、blends, and the second piece made of the fibre as indicated in Table 1 or, in the case of blends, of the kind of fibre second in order of predominance, or as otherwise specified. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E12
40、:1997 2 BSI 25 February 2003 Table 1 Single-fibre adjacent fabrics 4.3.3 If required, a non-dyeable fabric (for example, polypropylene). 4.4 Milling solution, containing 50 g of soap and 10 g of anhydrous sodium carbonate per litre. The soap shall contain not more than 5 % moisture and comply with t
41、he following requirements based upon dry mass: free alkali, calculated as Na2CO3: 0,3 % maximum; free alkali, calculated as NaOH: 0,4 % maximum; total fatty matter: 850 g/kg minimum; titre of mixed fatty acids prepared from soap: 30?C maximum; iodine value: 50 maximum. The soap shall be free from fl
42、uorescent whitening agents. 4.5 Test control, a dyeing of CI Acid Blue 7 (Colour Index, 3rd Edition) on wool fabric (see 8.2). 4.6 Grey scale for assessing change in colour, complying with ISO 105-A02, and grey scale for assessing staining, complying with ISO 105-A03. 4.7 Grade 3 water (see ISO 105-
43、A01:1989, subclause 8.2). 5 Test specimen 5.1 If the textile to be tested is fabric, either a) attach a specimen measuring 40 mm ? 100 mm to a piece of the multifibre adjacent fabric, also measuring 40 mm ?100 mm, by sewing along one of the shorter sides, with the multifibre fabric next to the face
44、of the specimen; or b) attach a specimen measuring 40 mm ?100 mm between the two single-fibre adjacent fabrics, also measuring 40 mm ?100 mm, by sewing along one of the shorter sides. 5.2 Where yarns or loose fibre is to be tested, take a mass of the yarn or loose fibre approximately equal to one ha
45、lf of the combined mass of the adjacent fabrics, and either a) place it between a 40 mm ?100 mm piece of the multifibre fabric and a 40 mm ?100 mm piece of the non-dyeable fabric and sew them along all four sides (see ISO 105-A01:1989, subclause 9.6) or b) place it between a 40 mm ?100 mm piece of e
46、ach of the two specified single-fibre fabrics and sew along all four sides. 5.3 Prepare the composite specimen of the test control (4.5) in the way outlined for fabric in 5.1. 6 Procedure 6.1 Carry out the operations described in 6.2, 6.3 and 6.4 with the composite specimen and the composite test-co
47、ntrol specimen in parallel, in separate baths. 6.2 Put the composite specimen and the composite test-control specimen in separate containers in the test device (4.1), each with three times its own mass of the milling solution (4.4) and 50 of the stainless-steel balls (4.2). Run the device for 2 h at
48、 40?C ?2?C. 6.3 Add sufficient grade 3 water (4.7) at 40?C ?2?C to give a liquor ratio of 100 : 1, and run the device for an additional 10 min. If first piece is:Second piece to be: cottonwool woolcotton viscosewool acetatewool polyamidewool polyesterwool acrylicwool Licensed Copy: sheffieldun sheff
49、ieldun, na, Sun Nov 19 13:38:58 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-E12:1997 BSI 25 February 2003 3 6.4 Remove the composite specimens, rinse twice in cold water (4.7) then rinse for 10 min in cold, running tap water. Open out the composite specimen (by breaking the stitching on all sides except one of the shorter sides, if necessary) and dry it by hanging it in air at a temperature not exceeding 60?C with the