《BS-EN-ISO-105-X04-1997.pdf》由会员分享，可在线阅读，更多相关《BS-EN-ISO-105-X04-1997.pdf（14页珍藏版）》请在三一文库上搜索。
1、BRITISH STANDARD BS EN ISO 105-X04:1997 Textiles Tests for colour fastness Part X04: Colour fastness to mercerizing (ISO 105-X04:1994) The European Standard EN ISO 105-X04:1997 has the status of a British Standard ICS 59.080.01 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:0
2、0 2006, Uncontrolled Copy, (c) BSI BS EN ISO 105-X04:1997 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 August 1997 BSI 10-1999 ISBN 0 580 27844 1 N
3、ational foreword This British Standard is the English language version of EN ISO 105-X04:1997. It is identical with ISO 105-X04:1994. It supersedes the relevent method in BS 1006:1990 which is withdrawn by amendment. The UK participation in its preparation was entrusted by Technical Committee TCI/25
4、, Chemical properties, to Subcommittee TCI/25/-/10, Colour fastness, which has the responsibility to: aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; mo
5、nitor related international and European developments and promulgate them in the UK. A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references Attention is drawn to the fact that Annex ZA lists normative references to international publica
6、tions with their corresponding European publications. The British Standards which implement these international or European publications may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index” or using the “Find” facility of the BSI Stand
7、ards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pag
8、es This document comprises a front cover, an inside front cover, pages i and ii, the EN ISO title page, page 2, the ISO title page, pages ii to iv, pages 1 and 2, an inside back cover and a back cover. This standard has been updated (see copyright date) and may have had amendments incorporated. This
9、 will be indicated in the amendment table on the inside front cover. Amendments issued since publication Amd. No.DateComments Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI BS EN ISO 105-X04:1997 BSI 10-1999i Contents Page National foreword
10、Inside front cover Foreword2 Forewordiii Text of ISO 105-X041 Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ii blank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EUROPEAN STANDA
11、RD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-X04 April 1997 ICS 59.080.01 Descriptors: See ISO document English version Textiles Tests for colour fastness Part X04: Colour fastness to mercerizing (ISO 105-X04:1994) Textiles Essais de solidit des teintures Partie X04: Solidit des teintures au mercer
12、isage (ISO 105-X04:1994) Textilien Farbechtheitsprfungen Teil X04: Farbechtheit gegen Mercerisieren (ISO 105-X04:1994) This European Standard was approved by CEN on 1997-03-28. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this Eu
13、ropean Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. The European Standards exist in three official versions (Englis
14、h, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Fin
15、land, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 B
16、russels 1997 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 105-X04:1997 E Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 BSI 10-1999 2 Foreword T
17、he text of the International Standard from Technical Committee ISO/TC 38 “Textiles” of the International Organization for Standardization (ISO) has been taken over as an European Standard by Technical Committee CEN/TC 248 “Textiles and textile products”, the secretariat of which is held by BSI. This
18、 European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 1997, and conflicting national standards shall be withdrawn at the latest by October 1997. According to the CEN/CENELEC Internal Regulations, th
19、e national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement
20、 notice The text of the International Standard ISO 105-X04:1994 has been approved by CEN as a European Standard without any modification. NOTENormative references to International Standards are listed in Annex ZA (normative). Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00
21、2006, Uncontrolled Copy, (c) BSI Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 ii BSI 10-1999 Contents Page Forewordiii 1Scope1 2Normative references1 3Principle1 4Apparatus and reagents1 5Test specimen1 6Procedure2 7Te
22、st report2 Annex ZA (normative) Normative references to international publications with their relevant European publicationsInside back cover Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 BSI 10-1999iii Foreword ISO (th
23、e International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committ
24、ee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechn
25、ical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard ISO 105-X04 was prepared by
26、Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. This fourth edition cancels and replaces the third edition (ISO 105-X04:1987), of which it constitutes a minor revision. ISO 105 was previously published in thirteen “parts”, each designated by a l
27、etter (e.g. “Part A”), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (e.g. “Section A01”). These sections are now being republished as separate documents, themselves designated
28、“parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in ISO 105-A01. Descriptors: Textiles, dyes, tests, chemical tests, mercerizing tests, determination, colour fastness. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006
29、, Uncontrolled Copy, (c) BSI iv blank Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 BSI 10-19991 1 Scope This part of ISO 105 specifies a method for determining the resistance of the colour of textiles to the action of
30、concentrated solutions of sodium hydroxide used in mercerizing. The method is mainly applicable to cotton and to mixtures containing cotton. 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisions of this part of ISO 105. At the
31、time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO 105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain
32、registers of currently valid International Standards. ISO 105-A01:1994, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. ISO 105-A03:1993, Textiles Tests for colour fa
33、stness Part A03: Grey scale for assessing staining. ISO 105-F:1985, Textiles Tests for colour fastness Part F: Standard adjacent fabrics. 3 Principle 3.1 A specimen of the textile in contact with a specified adjacent fabric is treated with sodium hydroxide solution, rinsed, acidified, rinsed again a
34、nd dried. The change in colour of the specimen and the staining of the adjacent fabric are assessed by comparison with the grey scales. 3.2 As completely resistant specimens may show an apparent increase in depth of colour, these cannot be rated 5 (no change) by the normal method of assessment. In s
35、uch cases, therefore, only the changes in hue and lightness can be assessed using the grey scale, without consideration of the increase in depth, and such assessments should be marked with an asterisk (*). The meaning of the asterisk should be explained in a footnote. EXAMPLES 5*: Increase in depth
36、(not considered); no change in hue and lightness. 34 redder*: Increase in depth (not considered); the hue became redder, matching grey scale 34. 2 bluer, duller*: Increase in depth (not considered); the shade changed in hue and lightness, matching grey scale 2. 3.3 Specimens whose colour does not in
37、crease in depth shall be assessed in the normal manner and the results shall not be marked with an asterisk. EXAMPLE 2 weaker, bluer, duller: Loss in depth (considered) and change in both hue and lightness corresponding to grey scale 2. 4 Apparatus and reagents 4.1 Cotton adjacent fabric, complying
38、with section F02 of ISO 105-F:1985, measuring at least 100 mm 100 mm, for evaluating staining. 4.2 Metallic frame, for holding specimen. A metal frame suitable for the test has two folding wings which can be locked in the closed position by a wing-nut. Each of the two wings is an open square of abou
39、t 80 mm 80 mm. All four sides of the frame are corrugated or contain needle bars in order to hold the composite specimen firmly during the treatment. The rigid frame for yarns and threads should be slightly larger than the corrugated or needle bar frame for fabrics and fit into the latter. 4.3 Sodiu
40、m hydroxide, aqueous solution, 300 g/l. 4.4 Sulfuric acid, aqueous solution containing 5 ml of concentrated sulfuric acid ( 1,84 g/ml) per litre. 4.5 Acetic acid, aqueous solution containing 10 ml of glacial acetic acid per litre. 4.6 Grey scale for assessing change in colour, complying with ISO 105
41、-A02, and grey scale for assessing staining, complying with ISO 105-A03. 5 Test specimen 5.1 If the textile to be tested is fabric, sew a specimen measuring at least 100 mm 100 mm to an equal-sized piece of the cotton adjacent fabric (4.1) around all four sides. Fasten this composite specimen to the
42、 frame (4.2) firmly, but without excessive tension. 5.2 If the textile to be tested is yarn or thread, wind an amount of it equal to the mass of the cotton adjacent fabric on a rigid frame firmly, but without excessive tension, with the strands close together and parallel to provide an area at least
43、 100 mm 100 mm. Sew an equal-sized piece of the cotton adjacent fabric (4.1) to this area along the two sides which cross the strands. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 2 BSI 10-1999 6 Procedure 6.1 Immerse
44、the composite specimen with the coloured material uppermost in the sodium hydroxide solution (4.3) at 20 C 2 C for 5 min. Rinse the composite specimen in the frame by pouring on it 1 litre of water at 70 C 2 C over a period of 1 min and then rinsing in cold, running tap-water for 5 min. 6.2 Remove t
45、he composite specimen from the frame and immerse in it the sulfuric acid solution (4.4) or in the acetic acid solution (4.5) for 5 min, at at liquor ratio of 50 : 1. Rinse the specimen in cold, running tap-water until neutral. 6.3 Remove the stitching along three sides of the specimen (one side for
46、yarns and threads) and dry it by hanging it in air at a temperature not exceeding 60 C, taking care that the adjacent fabric and the coloured material are kept apart except at the remaining stitching. 6.4 If the specimen shows increased depth of colour, assess the change in hue and/or lightness only
47、, using the appropriate grey scale (4.6). Assess the staining of the adjacent fabric by comparison with the appropriate grey scale (4.6). 6.5 If the specimen does not show increased depth of colour, assess the change as an overall contrast (see 3.3) and the staining of the adjacent fabric by compari
48、son with the grey scales. 7 Test report The test report shall include the following information: a) the number and year of publication of this part of ISO 105, i.e. ISO 105-X04:1994; b) all details necessary for the identification of the sample tested; c) in the case of assessments in accordance wit
49、h 6.4, any changes in hue and/or lightness of the specimen marked with an asterisk and the numerical grey scale rating for staining of the cotton adjacent fabric; d) in the case of assessments in accordance with 6.5, the numerical grey scale rating for change in colour of the specimen and the numerical grey scale rating for staining of the cotton adjacent fabric. Licensed Copy: sheffieldun sheffieldun, na, Sun Nov 19 13:24:46 GMT+00:00 2006, Uncontrolled Copy, (c) BSI EN ISO 105-X04:1997 BSI 10-1999 Annex ZA