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1、BRITISH STANDARD BS ISO 13678:2000 Incorporating Corrigendum No. 1 Petroleum and natural gas industries Evaluation and testing of thread compounds for use with casing, tubing and line pipe ICS 75.180.10 ? Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Co
2、py, (c) BSI BS ISO 13678:2000 This British Standard was published under the authority of the Standards Policy and Strategy Committee on 18 January 2006 BSI 15 March 2006 ISBN 0 580 36920 X National foreword This British Standard reproduces verbatim ISO 13678:2000, including Technical Corrigendum Oct
3、ober 2005 and implements it as the UK national standard. The UK participation in its preparation was entrusted to Technical Committee PSE/17, Petroleum and natural gases industries, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to i
4、ts secretary. Cross-references The British Standards which implement international publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue
5、or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the te
6、xt; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover,
7、 an inside front cover, the ISO title page, pages ii to v, a blank page, pages 1 to 35 and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. DateComments 16057 Corrigendum No. 1 15 March 2006Cor
8、rections to text Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Reference number ISO 13678:2000(E) INTERNATIONAL STANDARD ISO 13678 First edition 2000-12-01 Petroleum and natural gas industries Evaluation and testing of thread compounds for
9、 use with casing, tubing and line pipe Industries du ptrole et du gaz naturel valuation et essai des graisses de filetage utilises pour les tubes de cuvelage, les tubes de production et les tubes de conduites Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolle
10、d Copy, (c) BSI ISO 13678:2000(E) ii Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 13678:2000(E) iii Contents Foreword.iv Introduction.v 1Scope 1 2Normative references1 3Terms and definitions .1 4Thread compound characteristics.2 4.1Pr
11、oduct characteristics.2 4.2Physical and chemical characteristics2 5Thread compound performance properties6 5.1General6 5.2Frictional properties6 5.3Extreme surface-contact pressure (gall resistance) properties.7 5.4Fluid sealing properties 7 6Quality assurance and control.8 7Marking requirements .8
12、7.1Marking.8 7.2Labelling.8 Annex A (informative) API modified thread compound.9 Annex B (normative) Reference standard formulation .13 Annex C (normative) Penetration test.15 Annex D (normative) Evaporation test16 Annex E (normative) Oil separation test.17 Annex F (normative) Application/adherence
13、test18 Annex G (normative) Gas evolution test.19 Annex H (normative) Water leaching test.23 Annex I (informative) Frictional properties test .26 Annex J (informative) Extreme surface-contact pressure (galling) test28 Annex K (normative) Fluid sealing test.29 Annex L (informative) Corrosion inhibitio
14、n tests.32 Annex M (informative) Compound high-temperature stability test33 Bibliography34 Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 13678:2000(E) iv Foreword ISO (the International Organization for Standardization) is a worldwide
15、federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that c
16、ommittee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in acco
17、rdance with the rules given in the ISO/IEC Directives, Part 3. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention
18、is drawn to the possibility that some of the elements of this International Standard may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. International Standard ISO 13678 was prepared by Technical Committee ISO/TC 67, Materials, equipm
19、ent and offshore structures for petroleum and natural gas industries, Subcommittee SC 5, Casing, tubing and drill pipe. Annexes B to H and K form normative parts of this International Standard. Annexes A, I, J, L and M are for information only. Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27
20、07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 13678:2000(E) v Introduction This International Standard is based on API RP 5A3, first edition, June 1996. This International Standard specifies requirements and gives recommendations for the manufacture, testing and selection of thread compoun
21、ds for use on casing, tubing and line pipe based on the current industry consensus of good engineering practice. It is intended that the words casing and tubing apply to the service application rather than to the diameter of the pipe. The performance requirements of thread compounds for use with cas
22、ing, tubing and line pipe include: ?consistent frictional properties that will allow both proper and uniform connection engagement; ?adequate lubrication properties to resist galling or damage of connection contact surfaces during make-up and break-out; ?adequate sealing properties for thread type s
23、eal connections and/or not inhibiting the sealing properties of non-thread sealing connections (e.g. metal-to-metal seals, polytetrafluoroethylene (PTFE) seals, etc.) depending upon service requirements; ?physical and chemical stability both in service and in expected compound storage conditions; ?p
24、roperties that will allow effective application to the connection contact surfaces in expected service conditions and environment. When evaluating the suitability of a thread compound, the user should define the service conditions, and then consider field trials and field service experience in addit
25、ion to laboratory test results. Supplementary tests may be appropriate for specific applications which are not evaluated by the tests herein. The user and manufacturer are encouraged to discuss service applications and limitations of the compound being considered. Representatives of users and/or oth
26、er third party personnel are encouraged to monitor tests wherever possible. Interpolation and extrapolation of test results to other products, even of similar chemical composition, is not recommended. It should be recognized by the user that testing in compliance with this International Standard doe
27、s not in and of itself ensure adequate thread compound/connection system performance in field service. The user has the responsibility of evaluating the results obtained from the recommended procedures and test protocols and determining if the thread compound/connection system in question meets the
28、anticipated requirements of that particular field service application. Whether a thread compound meets local or global environmental legislation is outside the scope of this International Standard. However, it is the responsibility of the end user to be aware of the environmental requirements of the
29、 operating area and to select, use and dispose of the thread compound and related waste materials accordingly. Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Un
30、controlled Copy, (c) BSI INTERNATIONAL STANDARDISO 13678:2000(E) 1 Petroleum and natural gas industries Evaluation and testing of thread compounds for use with casing, tubing and line pipe 1Scope This International Standard provides requirements, recommendations and methods for the manufacture, test
31、ing and selection of thread compounds for use on ISO/API round thread, buttress thread and proprietary casing, tubing and line pipe connections. The tests outlined within this International Standard are used to evaluate the critical performance properties, and physical and chemical characteristics o
32、f thread compounds under laboratory conditions. These test methods are primarily intended for thread compounds formulated with a lubricating base grease. It is recognized that there may be materials used for the lubrication and/or sealing of threaded connections for which these test methods are not
33、applicable. This International Standard is not intended for the evaluation of compounds used with rotary shouldered connections. Such evaluation is described in API RP 7A1. This International Standard does not address the environmental issues associated with the use and disposal of thread compounds.
34、 2Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this International Standard. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreem
35、ents based on this International Standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC maintain registers
36、 of currently valid International Standards. ISO 2137:1985, Petroleum products Lubricating grease and petrolatum Determination of cone penetration. ISO 2176:1995, Petroleum products Lubricating grease Determination of dropping point. ISO 10400:1993, Petroleum and natural gas industries Formulae and
37、calculation for casing, tubing, drill pipe and line pipe properties. 3Terms and definitions For the purposes of this International Standard, the following terms and definitions apply. 3.1 seal barrier resisting the passage of fluids 3.2 thread compound substance that is applied to threaded oilfield
38、pipe connections prior to make-up to assist in their lubrication during assembly and disassembly and in their sealing against high internal and external pressures in service NOTESome thread compounds may also contain substances that provide storage compound properties. Licensed Copy: sheffieldun she
39、ffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 13678:2000(E) 2 3.3 storage compound substance that is applied to threaded oilfield pipe connections to protect against corrosion during either shipment or storage or both NOTECompounds that are for storage only should
40、not be used for connection make-up. 3.4 API modified thread compound compound designated as “modified thread compound” in API Bull 5A2 (obsolete). 3.5 reference standard thread compound that is formulated in accordance with the requirements of annex B, to include the limitations and tolerances in Ta
41、bles B.1, B.2 and B.3 NOTEThe reference standard is not intended for general field service. 3.6 connection pipe assembly consisting of two threaded male connection members (pins) and a coupling, or one pin and an integral female connection member (box) 3.7 thread compound/connection system system co
42、nsisting of the various critical threaded pipe connection components, including the specific connection geometry, and the individual connection materials and coatings combined with the thread compound 4Thread compound characteristics 4.1Product characteristics This International Standard outlines te
43、sts to characterize the performance of thread compounds under service conditions, rather than specifying the formulation. Thus, the purchaser and the manufacturer should agree on the product characteristics to be provided, such as: Thickener typeRheological properties Fluid typeCompound/copper react
44、ion AppearanceExtreme pressure properties Dropping pointFluid sealing properties Mass densityFrictional properties Oil separationCorrosion inhibition Flash pointBrushing/Adherence Water-absorption resistanceService applications Gas evolutionStorage and service life limitations The thread compound ma
45、nufacturer should publish timely product bulletins when any modification in formulation is implemented which would result in a change of any performance characteristic. All documentation shall provide data that are representative of a typical production batch. Test and inspection records generated u
46、nder this International Standard shall be retained by the manufacturer and shall be available to the purchaser for a minimum period of three years after the date of manufacture. 4.2Physical and chemical characteristics 4.2.1General The physical and chemical characteristics of performance-based threa
47、d compounds are specified in Table 1. These properties can vary widely, and the formulation of many of the available compounds is proprietary. Licensed Copy: sheffieldun sheffieldun, na, Mon Nov 27 07:21:32 GMT+00:00 2006, Uncontrolled Copy, (c) BSI ISO 13678:2000(E) 3 Therefore, the user should con
48、sider the performance properties and recommendations given by the compound manufacturers, in addition to the physical and chemical characteristics outlined in Table 1. Table 1 Thread compound physical and chemical characteristics tests PropertyTest methodPerformance value Dropping point, C (M)ISO 21
49、76138 min. (S) Evaporation, % volume fraction loss (M)See annex D 24 h at 100 ?C3,75 max. (S) Gas evolution, cm3(M)See annex G 120 h at 66 ?C20 max. (S) Oil separation, % volume fraction (M)See annex E 24 h at 100 ?C (nickel gauze cone)10,0 max. (S) Penetration, mm ? 101(M)See annex C Worked, 60 strokes at 25 ?C Production acceptability range (min. to max.)u 30 (S) Worked, 60 strokes at 7 ?CReport typical (R) Mass density, % variance (M)Manufacturers controls From production mean valu